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PET + ammonia. white powder
There's a whole thread on this somewhere on SM that followed from one members observasion that PET b ... |
18-1-2021 at 05:59
by: Boffis |
Preparation of Acetanilide
Very interesting Pumukli and another good write up.
Which reactions contained the "anhydride"? Is ... |
18-1-2021 at 01:40
by: Boffis |
furfural
I have now run two attempts at Fenton oxidation of xylitol (Fe2+ catalyzed H2O2 oxidation) and then ... |
16-1-2021 at 13:02
by: Boffis |
An attempt at making Phorone
I hate to say this but I think that chinese patent is garbage. Just look at how much energy is relea ... |
16-1-2021 at 10:53
by: Boffis |
Why are sulfuric acid ratios the same for nitrate salt and nitric acid?
They aren't and you can't generalize aout such things but you are probably looking at ill designed a ... |
16-1-2021 at 06:37
by: Boffis |
C.T.M.T.N.A (R-salt)
Regarding the stability of this compound, I have just come across the jar of recrystallised material ... |
16-1-2021 at 04:14
by: Boffis |
An attempt at making Phorone
Hi EverythingAl2O3, I've been following your experimental endeavors with interest as I have been con ... |
15-1-2021 at 15:27
by: Boffis |
mononitrotoluenes (nitration of toluene)
Ahh. That is interesting. I presume you recovered your toluene from some solvent type material. I wo ... |
15-1-2021 at 11:54
by: Boffis |
mononitrotoluenes (nitration of toluene)
Hi Fery, another nice write up. I haven't tried this preparation for over 30 years but I don't remem ... |
13-1-2021 at 13:59
by: Boffis |
1,4-naphtoquinone by naphtalene oxidation with dichromate
Interesting work Fery, and a nice write-up even if not 100% successful! I had been thinking about tr ... |
13-1-2021 at 10:39
by: Boffis |
furfural
While emptying out the flask from one of the reaction I found these beautiful hopper salt crystals i ... |
11-1-2021 at 15:11
by: Boffis |
Mercury selenite
Well, this is what my samples look like: mercury selenite, tellurite and tellurate,
[file]85977[ ... |
11-1-2021 at 13:16
by: Boffis |
Fenton type oxidation
Tried this again with 25g of xylitol, 220ml of 3% H2O2 that's a higher ratio of H2O2 to xylitol than ... |
11-1-2021 at 12:20
by: Boffis |
Friedel-Crafts acylation of anilides
Thanks njl, that is interesting!
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11-1-2021 at 12:15
by: Boffis |
Friedel-Crafts acylation of anilides
That is interesting, if it works with p-chloroacetyl chloride I can see no reason why it should not ... |
11-1-2021 at 07:55
by: Boffis |
Mercury selenite
Hi Vano, Many years ago I acquired a collection of mercury compounds from a guy who had worked on th ... |
11-1-2021 at 06:59
by: Boffis |
Fenton type oxidation
Thanks for the information Sedit!!
I have tried Fenton's type oxidations before and had variable ... |
10-1-2021 at 04:14
by: Boffis |
Friedel-Crafts acylation of anilides
Tricky  , As we say "the Devil is in the detail"
If you mix the acetanilide with the acetylation ... |
9-1-2021 at 15:39
by: Boffis |
Friedel-Crafts acylation of anilides
Hi Pumukli, take a look at these two papers:
Chattaway, Proc. Chem. Soc. 1902, p173 and 1903, p12 ... |
9-1-2021 at 12:58
by: Boffis |
Fenton type oxidation
Does anyone have any actual experience of the se of Fenton's reagent in oxidation in organic chemist ... |
9-1-2021 at 02:18
by: Boffis |
Successful Synthesis of 1-Amino-3-nitroguanidine Nitrate
Did you check out this thread?:
http://www.sciencemadness.org/talk/viewthread.php?tid=83736 |
8-1-2021 at 14:46
by: Boffis |
Things to do with Ethyl Formate
[rquote=652755&tid=156492&author=Pumukli]Why not combine the two? Alkaline sulfide precipita ... |
8-1-2021 at 09:04
by: Boffis |
Things to do with Ethyl Formate
I have now isolated over 60g of copper triazole sulphate, its composition is as yet unknown but look ... |
8-1-2021 at 03:35
by: Boffis |
p-Nitroso-dimethylaniline
Hi Pumukli, I had a go at recrystallising some of my least pure p-nitrosodimethylaniline from pet et ... |
7-1-2021 at 14:39
by: Boffis |
Group buy Duran Keck vacuum erlenmeyer adapters
Thanks Bubbles. Glad to hear they arrived OK. |
7-1-2021 at 13:53
by: Boffis |
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