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Pyrollidine smell from amino acid & Mg ribbon Seems plausible that you're just generating a lot of heat at the reaction surface leading to thermal ...	18-1-2023 at 09:50 by: clearly_not_atara
Not really iron? Remember that story about Archimedes and the crown?	7-1-2023 at 13:38 by: clearly_not_atara
Purification of Cobalt solution (sulphate/Chloride) If you form the cobalt ammine complex, you can precipitate Co(NH3)6Br3 with high efficiency. You nee ...	6-1-2023 at 10:27 by: clearly_not_atara
Cesium production from new method I'm certain that you could heat a mixture of CsCl and iron filings until the latter melts and you st ...	5-1-2023 at 17:59 by: clearly_not_atara
Synthesis of 3,4,5-trimethoxy cinnamic acid using green Knoevenagel condensation I don't think that malonic acid will "fit", sterically, but the Reformatsky reaction should be a go.	4-1-2023 at 20:24 by: clearly_not_atara
Other acids than oxyacids The reason that practically all of the covalent acids are oxoacids is that the other elements would ...	2-1-2023 at 08:10 by: clearly_not_atara
OTC arylboronic esters Sometimes the abstract says everything. [i]A novel preparation of aryl and heteroarylboronic acids ...	30-12-2022 at 21:38 by: clearly_not_atara
What can i make from this compounds? I found this thread again because I had identified diphenyl sulfone (lit bp 374 C) as a possible hig ...	28-12-2022 at 11:31 by: clearly_not_atara
How to tell borosilicate from non-borosilicate glass Just get a source of thermal neutrons and measure the absorption cross-section. Borosilicate will de ...	22-12-2022 at 11:00 by: clearly_not_atara
Cheapest Hydroxylamine [quote]and SO3 is bubbled through the agitated reaction mixture[/quote] Surely he means to say "an ...	21-12-2022 at 13:52 by: clearly_not_atara
Can DCM act as a Lewis Acid? You have AlCl3 in your system. So there's obviously a Lewis acid present! But maybe you meant to say ...	20-12-2022 at 17:33 by: clearly_not_atara
AlCl3 by double displacement? [rquote=679523&tid=159094&author=blogfast25] Also if it was possible to oxidise Al 0 to Al+ ...	19-12-2022 at 11:38 by: clearly_not_atara
Magnesium chromate from electrolysis of stainless steel in magnesium sulphate solution [rquote=679485&tid=159153&author=blogfast25] That would be an interesting tidbit but really ...	17-12-2022 at 13:05 by: clearly_not_atara
AlCl3 by double displacement? Ammonium tetrachloroaluminate is described as melting cleanly 303 C: https://pubs.acs.org/doi/pdf/1 ...	17-12-2022 at 12:53 by: clearly_not_atara
AlCl3 by double displacement? AlCl3 is a Friedel-Crafts catalyst. Refluxing it in xylene or toluene will cause (slow) disproportio ...	14-12-2022 at 21:28 by: clearly_not_atara
New chemical restrictions in Canada? [rquote=662534&tid=157676&author=S.C. Wack][rquote=662524&tid=157676&author=Fyndium] ...	14-12-2022 at 10:18 by: clearly_not_atara
AlCl3 by double displacement? I am certain that AlCl3 forms a complex with NH3. Not sure how easy it is to break — maybe just Ts ...	14-12-2022 at 07:59 by: clearly_not_atara
Interesting route to 4-methoxyphenol I would be interested to find out what the nitrosation product of paracetamol is. If you get N-nitra ...	14-12-2022 at 07:41 by: clearly_not_atara
AlCl3 by double displacement? On further consideration, CuCl should give a much less exothermic process than CuCl2. And it's insol ...	9-12-2022 at 13:37 by: clearly_not_atara
Positive Iodine Compounds You could possibly use hexammine cobalt (III) acetate. (NH3)6CoBr3 has a very low solubility in wate ...	6-12-2022 at 21:24 by: clearly_not_atara
Confusion on SO3 Synthesis I've often wondered if there was a way to directly acidify pyrosulfate. Unfortunately, disulfuric ac ...	4-12-2022 at 11:35 by: clearly_not_atara
Preparation of ionic nitrites I would cross my fingers too when heating a flammable solvent with a somewhat unstable oxidant...	3-12-2022 at 17:43 by: clearly_not_atara
can hydrogen be stored under low pressure for hydrogenation reactions? Nickel-catalysed isopropanol-donor CTH can reduce alkenes with the assistance of ultrasound: http ...	2-12-2022 at 08:18 by: clearly_not_atara
Preparation of chlorosulfonic acid derived protecting groups I'm not aware of any way to make TsCl from SO2Cl2, either. Friedel-Crafts conditions will give mostl ...	1-12-2022 at 14:59 by: clearly_not_atara
Hydrolysis of alkyl halides This is not hydrolysis, it's called hydrogenolysis. But see: https://pubs.acs.org/doi/10.1021/ja0 ...	1-12-2022 at 06:36 by: clearly_not_atara
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