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KCLO3 by way of H2O + KCL
Xenoid said

[quote]If you are making your first chlorate cell, graphite or carbon "gouging rods" ...
27-8-2007 at 09:00
by: DerAlte
What would you call a real chemical?
YT2095 is right. Purely subjective. I'd say something in a bottle that is not a mixture, but a reage ...
25-8-2007 at 09:31
by: DerAlte
Permanganates
I've had this post on the back burner but I’ve been too interested in the possibilities of an ele ...
24-8-2007 at 22:50
by: DerAlte
Permanganates
@not_important: agree absolutely about getting rid of the carbon and the iron. I show how to earlier ...
24-8-2007 at 22:45
by: DerAlte
Permanganates
Great try, Xenoid! Your turn around time is spectacular and your set up looks highly professional. I ...
24-8-2007 at 19:37
by: DerAlte
Permanganates
I have read the patent. I have the following comments:

(1) No diaphragm is mentioned. No deta ...
24-8-2007 at 12:39
by: DerAlte
Permanganates
It sounds a nasty brew, but in my (small) experience as an amateur, I think the erosion of glass by ...
23-8-2007 at 17:21
by: DerAlte
Permanganates
To balance it,

MnO2 + KNO3 + 2KOH => K2MnO4 + KNO2 + H2O

In the fusion method, yes. It won ...
23-8-2007 at 13:49
by: DerAlte
storing KCN
If you can't smell it there's either none there or too much - in which case it may be too late! This ...
23-8-2007 at 09:02
by: DerAlte
Permanganates
Xenoid, very interesting! Your set up is just about what I was thinking of, bar the carbon anode. I ...
23-8-2007 at 08:52
by: DerAlte
Permanganates
@ [b]ciscosdad[/b] Very much so! I had been thinking and an MnO2 anode (somehow encased) in a diaph ...
22-8-2007 at 20:57
by: DerAlte
Indole
Skatole is 3-methyl indole, responsible for the odor of feces. Indole itself also smells foul unless ...
19-8-2007 at 13:40
by: DerAlte
Permanganates
@Rosco - had a quick look at that thread. It seemed to me from Hilski's excellent photos that in fac ...
19-8-2007 at 12:01
by: DerAlte
Permanganates
@ Xenoid - having trouble with U2U, have read your message but failed to reply successfully. I haven ...
19-8-2007 at 09:22
by: DerAlte
Permanganates
@ Ballermatz - good video! I assume the decomposition is something like:

2NH4MnO4 --> N2 + 4H2 ...
17-8-2007 at 13:35
by: DerAlte
Rare earth metals, mischmetal, etc
Just a few final notes. I used magnesium sulphate heptahydrate finely ground as a source of SO4-- io ...
17-8-2007 at 13:05
by: DerAlte
Montmorillonite Clay as Desiccant
Great info., [b]not_important[/b]! Added to my pile... Der Alte
17-8-2007 at 12:53
by: DerAlte
Montmorillonite Clay as Desiccant
Thanks! Sounds like it behaves much like silica gel. Those graphs were rather useful, not_important. ...
15-8-2007 at 23:00
by: DerAlte
Permanganates
ALTERNATIVE METHODS OF PERMANGANATE PREPARATION....

(1)The alkali + oxidant method – see the va ...
15-8-2007 at 22:51
by: DerAlte
Montmorillonite Clay as Desiccant
Anyone ever heard of this 'Activated Clay' as a dessicant? I got a bag (about 2 oz.) of this stuff ...
13-8-2007 at 22:20
by: DerAlte
Rare earth metals, mischmetal, etc
SULPHATES FINALLY EXTRACTED AND PURIFIED

Finally got around to it.

The Ce2(SO4)3 went off in ...
13-8-2007 at 22:11
by: DerAlte
Alarmism first! - reality check later on...
@ Rosco Bodine - I am on your wavelength, as you probably realized by now. However, who ever cared ...
11-8-2007 at 23:22
by: DerAlte
Permanganates
@ Filemon

You have the gist of a method, but using NaOH in the manner you suggest will raise the ...
11-8-2007 at 21:53
by: DerAlte
oxidation alcohol to aldehyde with MnO2
I don't think Mn++ ions will be oxidized to MnO2 by an alkali nitrate at high pH. NO3- is a rather w ...
9-8-2007 at 18:50
by: DerAlte
Rare earth metals, mischmetal, etc
@ The_Davster:-

The color of Ce++++ noted - and I've seen it since so described else where - so ...
9-8-2007 at 17:53
by: DerAlte
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