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Beta-Alanine amino acid copper salt
I'm not sure if chirality is the right term, but that type of isomerism can actually effect reaction ...
17-2-2021 at 11:02
by: njl
Benzoyl chloride + 4-Aminoadamantan-1-ol
No specific ref, but I think that once the amine salt is formed the alcohol can be halogenated a la ...
16-2-2021 at 07:15
by: njl
Benzoyl chloride + 4-Aminoadamantan-1-ol
Maybe chlorinate with HCl to get 4-Aminoadamantan-1-chloride, followed by reaction with sodium benzo ...
14-2-2021 at 19:27
by: njl
Benzoyl chloride + 4-Aminoadamantan-1-ol
The amine shown in the procaine synthesis is tertiary so it can't be acylated by benzoyl chloride, 4 ...
14-2-2021 at 14:28
by: njl
NiCl2 Weirdness
@Lion will do.

@Boffis lighten up a little... it's impossible to over engineer something done pur ...
14-2-2021 at 07:51
by: njl
NiCl2 Weirdness
I'm having some trouble with a batch of nickel chloride I just made. I did not follow a procedure re ...
13-2-2021 at 10:48
by: njl
Acetic anhydride preparation
Can't remember where but I think I remember a prep for isopropenyl acetate that involved bubbling MA ...
11-2-2021 at 05:51
by: njl
Acetic Anhydride from Zinc Acetate?
It would have cost you nothing to not say that.
9-2-2021 at 09:12
by: njl
A new way to make NCl3?
Yeah, but the chlorination of ammonia is the standard method for NCl3. How is this new?
9-2-2021 at 08:16
by: njl
Isocyanate synthesis via halide displacement
True. I wasn't planning on trying this anytime soon. Perhaps alkyl halide in acetone, dripped into a ...
8-2-2021 at 13:38
by: njl
Black Phosphorus Sources
https://sci-hub.st/http://dx.doi.org/10.1039/C9TA13441G
8-2-2021 at 09:58
by: njl
Isocyanate synthesis via halide displacement
Silver cyanate seems like a logical starting point given the insolubility of silver halides.

http ...
8-2-2021 at 09:20
by: njl
Acetic Anhydride from Zinc Acetate?
[rquote=654507&tid=156991&author=Fyndium]
Personally, I have access to a lathe, a mill and ...
8-2-2021 at 07:55
by: njl
Reaction of Ammonium Chloride and Sodium Bicarbonate
NH4Cl forms an acidic solution. If this solution is mixed with aq NaHCO3, CO2 will be released and t ...
6-2-2021 at 07:20
by: njl
Can you make bromine in the separatory funnel?
Shaking with H2SO4 is common
5-2-2021 at 14:54
by: njl
My hydroxylamine smells like cyanide
This is really interesting... even if you did have iron salts, would those salts be reduced by hydro ...
5-2-2021 at 07:42
by: njl
Can you make bromine in the separatory funnel?
Similar idea, would an electrobromine cell in an addition funnel be advantageous? Anode at the botto ...
5-2-2021 at 07:07
by: njl
Acetic Anhydride from Zinc Acetate?
On the acetic anhydride thread this concept has been brought up a couple times and each time it gets ...
5-2-2021 at 07:04
by: njl
Most toxic compound OTC?
I don't really follow Fyndium. Sounds like their point stands, if you don't know what you're doing y ...
2-2-2021 at 06:50
by: njl
Methaqualone
The salt is probably more stable than the freebase.
2-2-2021 at 06:37
by: njl
Acylal and "ketylal" properties
Bump because this is cool :P

I found one paper that has some practical info:
https://insa.nic.in ...
2-2-2021 at 06:32
by: njl
Calcinated Erbium & Chromium Oxide - new options?
Try NaOH with your Cr2O3 to get hexahydroxychromate, then perhaps you could recrystallize and acidif ...
1-2-2021 at 08:33
by: njl
Acylal and "ketylal" properties
Can anyone link any literature regarding the synthesis and reactivity of "Acylals" and "Ketylals" (g ...
1-2-2021 at 07:22
by: njl
Calcinated Erbium & Chromium Oxide - new options?
Which oxides are you referring to? And what is your goal?
1-2-2021 at 07:05
by: njl
Problem using Chloroacetyl Chloride
I totally agree most things are blown out of proportion for amateurs, but the effects of BzCl is not ...
1-2-2021 at 07:00
by: njl
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