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Benzyl chloride from Benzyl acetate
DJF90 - As mentioned earlier in the post, i have just bought ~2 litres of benzyl acetate, BDH A.R. a ...
27-12-2009 at 07:03
by: Picric-A
Benzyl chloride from Benzyl acetate
I use my refractometer (bought of ebay for £30 :D) similar to this one:
http://cgi.ebay.co.uk/Abbe ...
26-12-2009 at 14:52
by: Picric-A
Benzyl chloride from Benzyl acetate
[rquote=168165&tid=13162&author=entropy51]Gee, who would ever have thought this would work?[ ...
26-12-2009 at 14:30
by: Picric-A
Benzyl chloride from Benzyl acetate
I did a B.P test to identify it then fractionated it with a 60cm fractionating column, finally measu ...
26-12-2009 at 11:30
by: Picric-A
Benzyl chloride from Benzyl acetate
Wrong, sorry. I have taken everything you say into account and have 200ml of very poure Benzyl alcoh ...
26-12-2009 at 04:22
by: Picric-A
Merry Christmas Everybody!!!!!!!!
24-12-2009 at 16:00
by: Picric-A
Benzyl chloride from Benzyl acetate
@ smuv- we are not trying to 'decompose' the ester, we are trying to hydrolyse (saponify) it, ie, we ...
24-12-2009 at 14:51
by: Picric-A
Benzyl chloride from Benzyl acetate
I never said i didnt want to try research, i said i didnt want to try something new with cyanides.
...
24-12-2009 at 09:31
by: Picric-A
nitroglycerin
Add a couple of drops of washing liquid solution to the NG drops, should cause them to drop.
24-12-2009 at 03:15
by: Picric-A
Benzyl chloride from Benzyl acetate
[rquote=167988&tid=13162&author=Nicodem][rquote=167979&tid=13162&author=Picric-A]Hmm ...
24-12-2009 at 02:45
by: Picric-A
Concentrations of a few "Household" Chemicals
The Drain unblocker we buy in the UK ( i buy from Wilkinsons) has written on the label itself "95% S ...
23-12-2009 at 17:54
by: Picric-A
Benzyl chloride from Benzyl acetate
Hmm... well i guess the acetate leaving group is out of the question...

Back to hydrolysis to the ...
23-12-2009 at 17:49
by: Picric-A
Benzyl chloride from Benzyl acetate
That is true for aliphatic primary + secondary alcohols but according to the site aromatic alcohols ...
23-12-2009 at 01:24
by: Picric-A
Benzyl chloride from Benzyl acetate
I have recently bought 2l of Benzyl acetete off ebay for 99p (yep 99p :) ) and i plan to do somethin ...
22-12-2009 at 03:13
by: Picric-A
Reactions in a 'Sealed Tube'
Nice attachment Ozone, thanks.

@Entropy - I am indeed attempting to prepare 2-butanamine from 2-c ...
17-12-2009 at 04:07
by: Picric-A
Reactions in a 'Sealed Tube'
Several reactions i have come across, such as condensations ect. are required to be performed in a s ...
16-12-2009 at 14:54
by: Picric-A
Phosphoryl Halides - From P4O10 & Halide Salts
Interesting collection of articles, have you done any experimentation with these yourself?
16-12-2009 at 02:38
by: Picric-A
Drug discovery related informations
Awsome blog medchem! i Especially like the page of Baloon hydrogenation, awsome vid!
Thanks!
14-12-2009 at 03:48
by: Picric-A
Frozen reagent bottle stopper
I managed to open both stopper.
I applied some WD40 to the stopper and left for 10 mins to seep in ...
12-12-2009 at 06:13
by: Picric-A
Frozen reagent bottle stopper
[rquote=167035&tid=13110&author=stateofhack]Use your teeth :D[/rquote]

might give it a sh ...
8-12-2009 at 10:56
by: Picric-A
Frozen reagent bottle stopper
I have tried the wooden tapping with no success...
i was just rightly scared to heat a bottle of ni ...
8-12-2009 at 08:48
by: Picric-A
Frozen reagent bottle stopper
I considered using a penetrating solvent or grease but i dont want to contaminate my 99p bottle of n ...
8-12-2009 at 02:41
by: Picric-A
Frozen reagent bottle stopper
I have just bough some rather old yet full bottles of Nitrobenzene, Acetic acid and Benzyl acetate a ...
8-12-2009 at 00:18
by: Picric-A
Preparation of cyanides
It scares me when new members ask questions regarding the preperation of 'liquid hydrogen cyanide'.. ...
4-12-2009 at 12:08
by: Picric-A
Hardware store chemicals - questions
Try bubbling a bit of H2S through the PbSO4/H2SO4, then chill to Ppt PbS.
Filter though glass and y ...
3-12-2009 at 11:46
by: Picric-A
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