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4,7-phenanthroline-5,6-dione intermediate
start off with 3-nitroanisole(you could start with 3-nitrophenol,but better to avoid the methylatio ...
11-12-2016 at 06:03
by: CuReUS
n n-diethylmethylamine synthesis
[rquote=468582&tid=71192&author=careysub]DEET (N,N-Diethyl-meta-toluamide) is generally a mo ...
10-12-2016 at 00:13
by: CuReUS
n n-diethylmethylamine synthesis
[rquote=468578&tid=71192&author=Aqua-regia]Bad news, but eschweiler on DEA needs superatmosp ...
9-12-2016 at 10:26
by: CuReUS
Preparation of Succinic Acid
why not make succinic acid from MSG using a mixture of H[sub]2[/sub]O[sub]2[/sub] and HClO[sub]2[/su ...
9-12-2016 at 07:28
by: CuReUS
n n-diethylmethylamine synthesis
No need to jump to the nuclear option just yet.;),Why not try an eschweiler-clarke on diethylamine f ...
9-12-2016 at 06:35
by: CuReUS
Benzene ---> Phenol
previously,the direct hydroxylation of arenes was done by fenton's reagent.But the reaction is messy ...
4-12-2016 at 08:04
by: CuReUS
Cis/Trans isomerism of alkane 1,2 diol
See this paper, they use GC retention time and mass spectra to prove that the stereochemistry was tr ...
4-12-2016 at 05:13
by: CuReUS
The Short Questions Thread (4)
[rquote=468138&tid=25055&author=gluon47] I am unsure if isopropylamine reacts with calcium c ...
3-12-2016 at 21:06
by: CuReUS
dioxane gunk removal
[rquote=468077&tid=70330&author=dactyl]The dissolution in piranha acid seem slow to a degree ...
3-12-2016 at 05:25
by: CuReUS
What could one do with ICl?
why not try using sodium dithionite as the reducing agent ? or H[sub]2[/sub]O[sub]2[/sub] in alkalin ...
3-12-2016 at 05:16
by: CuReUS
Author asking for basic chemistry ideas for fiction.
a few days back,I was watching a show called-"doomsday:10 ways the world will end" and the episode w ...
3-12-2016 at 00:53
by: CuReUS
NaBH4 to Na triacetoxyborohydride
See this -[url]http://www.sciencemadness.org/talk/viewthread.php?tid=7744&goto=search&pid=87 ...
1-12-2016 at 08:51
by: CuReUS
p-Dichlorobenzene and Ferric Chloride
To have even more fun,why go via the straight forward FeCl[sub]3[/sub]/Cl[sub]2[/sub] route which is ...
30-11-2016 at 01:20
by: CuReUS
Trying to synthesize 1-iodobutane
[rquote=467633&tid=70660&author=NitratedKittens]Could HCl + KI + Butanol work[/rquote]
[rqu ...
28-11-2016 at 02:15
by: CuReUS
Fluoroantimonic + Hydrogen Peroxide Reaction?
[rquote=467576&tid=70617&author=stoichiometric_steve]
It's an aqueous solution[/rquote]
fr ...
28-11-2016 at 01:30
by: CuReUS
Fluoroantimonic + Hydrogen Peroxide Reaction?
you can find the answer in this video -[url]https://www.youtube.com/watch?v=N3xyICmQHy8[/url]

[Edit ...
26-11-2016 at 23:18
by: CuReUS
Benzylamine via the delepine reaction
You are correct,you will get some benzaldehyde as by product.You will also get some NH[sub]3[/sub] a ...
26-11-2016 at 23:11
by: CuReUS
carboxylic acid and thionyl chloride question
why not just use good old TCT ? [url]http://chemistry.mdma.ch/hiveboard/novel/000372508.html[/url]

...
26-11-2016 at 03:52
by: CuReUS
anti suck back valve
Myst32 has a brilliant video about a home made anti suck back apparatus -[url]https://youtu.be/kqQ ...
25-11-2016 at 00:00
by: CuReUS
stork reaction amine alternatives?
What are you trying to synthesise ? (CAS no please). Surely there must be better ways to alkylate ke ...
23-11-2016 at 05:45
by: CuReUS
Production of H2SO4 from burning coal? SO2 + O2 + H2O?
The contact process needs a catalyst,which can get poisoned due to the impurities in the coal exhaus ...
22-11-2016 at 04:53
by: CuReUS
Keeping polypropylene sheets soft and flexible after autoclaving.
diethylhexyl phthalate is used for softening vinyl gloves,so you could try that.
21-11-2016 at 08:26
by: CuReUS
Need help with a pH problem.
I am getting K[sub]a[/sub] as 4.63 * 10[sup]-5[/sup]

[Edited on 20-11-2016 by CuReUS]
20-11-2016 at 08:00
by: CuReUS
Benzylamine via the delepine reaction
you don't have to use CHCl[sub]3[/sub],any solvent that will dissolve the adduct will do.Alcohol and ...
19-11-2016 at 23:46
by: CuReUS
Briggs–Rauscher reaction - Chemical Oscillations
the wiki page clearly explains why malonic acid is used and also gives alternatives.But why don't yo ...
18-11-2016 at 07:41
by: CuReUS
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