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Possible OTC, 'safe' methylating agents
***Never mind, misunderstood!

[Edited on 2-15-2020 by monolithic]
15-2-2020 at 12:35
by: monolithic
Possible OTC, 'safe' methylating agents
[rquote=631061&tid=11580&author=horribilis][rquote=631054&tid=11580&author=wakatutu] ...
14-2-2020 at 15:05
by: monolithic
Does anyone know if these are borosilicate or not?
[rquote=631042&tid=154859&author=Ludus]when I started out I bought almost all my labware fro ...
14-2-2020 at 06:48
by: monolithic
Does anyone know if these are borosilicate or not?
I imagine they are borosilicate but I'm not 100% sure. The vegetable oil index of refraction trick s ...
11-2-2020 at 04:15
by: monolithic
Possible OTC, 'safe' methylating agents
[rquote=630851&tid=11580&author=clearly_not_atara]I think it could probably work, diglyme's ...
10-2-2020 at 18:57
by: monolithic
Possible OTC, 'safe' methylating agents
Slightly off topic, slightly on topic: any thoughts on whether dimethyl carbonate could be used to m ...
10-2-2020 at 17:50
by: monolithic
Is it cheaper to buy or make hot plate magnetic stirrers?
The cheap Chinese/Indian ones are mostly garbage that can barely boil water. You can build one yours ...
10-2-2020 at 17:20
by: monolithic
Stir plate magnet strength?
[rquote=630775&tid=154848&author=Deathunter88]Check your stir bar first, they get demagnetiz ...
9-2-2020 at 14:37
by: monolithic
Stir plate magnet strength?
I own a Corning PC-351 and I like it aside from the stir plate magnet,which seems to be a bit weak. ...
9-2-2020 at 10:17
by: monolithic
Best materials for chemical work surfaces?
Soapstone is the "classic" chemistry bench top material.
9-2-2020 at 05:56
by: monolithic
a new OTC Mukaiyama-like coupling reagent from thiamin?
Can you dumb it down for me and show some examples of what this reagent can do? :D
9-2-2020 at 05:55
by: monolithic
Made to order PTFE adapters
[rquote=630739&tid=144230&author=draculic acid69]Once again we've all been left hanging.lopt ...
8-2-2020 at 17:35
by: monolithic
Made to order PTFE adapters
Could you make a 24/40 rotary joint for a DIY rotovap?
8-2-2020 at 11:54
by: monolithic
Cheap OTC DCM in the USA?
For anyone wondering, Dural will not ship DCM to a residential address. Man of Ohm will not ship DCM ...
21-1-2020 at 16:29
by: monolithic
Solvents for acid/base workups of amines?
I've used chloroform on tertiary amines, worked great. No clue about primary amines.

[rquote=6297 ...
20-1-2020 at 17:02
by: monolithic
Emulsions from MgSO4?
[rquote=629411&tid=154719&author=AvBaeyer]At the risk of being reprimanded I will ask: You a ...
13-1-2020 at 04:14
by: monolithic
Can amateurs buy thionyl chloride from www.chemsavers.com?
I believe if it's anything questionable, which probably includes SOCl3, you have to fill out an inte ...
12-1-2020 at 15:58
by: monolithic
Emulsions from MgSO4?
[rquote=629390&tid=154719&author=Dr.Bob]It may just have fines in the mix, MgSO4 is the fluf ...
12-1-2020 at 14:54
by: monolithic
Emulsions from MgSO4?
I get a persistent white emulsion every time I dry a compound with a particular brand of MgSO4. The ...
12-1-2020 at 14:30
by: monolithic
Crystallization Techniques
When you've added enough boiling solvent to reach saturation (plus a bit more), turn your hot plate ...
12-1-2020 at 08:22
by: monolithic
Kitchenware Pyrex on Hotplate
I think I've used those exact style Pyrex bowls on my ceramic hot plate to run hot oil baths up to 1 ...
22-12-2019 at 05:55
by: monolithic
Magpie has died
He will be missed. Reading his posts was always a joy.
14-12-2019 at 07:16
by: monolithic
Allyl Bromide Preparation
Nice work. Plan on doing a write up on the impending Grignard reaction? :)
11-12-2019 at 16:41
by: monolithic
Diethylamine hydrochloride - Success!
[rquote=626921&tid=154467&author=chemist1243]
are you sure? ive hear diethyl ether is prett ...
27-11-2019 at 14:51
by: monolithic
Diethylamine hydrochloride - Success!
[rquote=626816&tid=154467&author=Pumukli]Monolithic: I doubt if it was. Such assymetric amin ...
27-11-2019 at 06:41
by: monolithic
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