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3,4-dihydroxy-5-methoxybenzaldehyde synthesis
Hey thanks for the responses.
Currently I am recrystallizing .75gr of the crude material from a 1to ... |
7-10-2010 at 10:17
by: mnick12 |
3,4-dihydroxy-5-methoxybenzaldehyde synthesis
Well I thought I would share my attempt at synthesizing 3,4dihydroxy-5-methoxybenzaldehyde from 5-br ... |
6-10-2010 at 20:21
by: mnick12 |
The short questions thread (3)
Does anyone know if 5-hydroxyvanillin has a distinct odor?
The reason why I ask is I attempted the ... |
5-10-2010 at 11:52
by: mnick12 |
NH4NO3 rendition of psuedo-Birch reduction
There has been some work done on lithium bronze by me and others.
I believe the cooks use it becaus ... |
4-10-2010 at 10:21
by: mnick12 |
Odd results from 5-bromovanillin synthesis?
Ahh well a little update,
So after sitting for an hour I added 200ml of water causing the precipi ... |
2-10-2010 at 13:01
by: mnick12 |
Odd results from 5-bromovanillin synthesis?
Well I have a question regarding the bromination of vanillin using elemental bromine, vanillin, and ... |
1-10-2010 at 17:54
by: mnick12 |
overheating hotplate with Al foil?
It depends on how strong of a vacuum your pulling. Generally speaking it is advised to use a rbf whe ... |
25-9-2010 at 17:25
by: mnick12 |
Tutorial for making a miniature chlorate cell
Now I know this is not directly related, but it is similair and does not deserve its own thread. Reg ... |
25-9-2010 at 10:55
by: mnick12 |
Anorganic peroxides
Well BaO2 is pretty cheap it can be bought from pyro suppliers. As for BaSO4 flash powder, BaSO4 alo ... |
21-9-2010 at 17:13
by: mnick12 |
5-ATZ(5-Aminotetrazole), the nitrotetrazolate ion and friends
Well today I thought I would test some 5-atz.
I mixed a small amount of 5-atz with enough ethylen ... |
19-9-2010 at 17:59
by: mnick12 |
ground glass joint help
I know this is not what you asked for, but it has always worked in my experience.
Well I had a si ... |
18-9-2010 at 19:14
by: mnick12 |
atx psu problems....
I had the same problem with one of my psu supplies. Most of the newer models have a "load sense", so ... |
17-9-2010 at 22:25
by: mnick12 |
Oxidizing alcohols for beginners - Making oxidizing agent
Well it all depends on what you have available as well as what you want. My question is, what is you ... |
13-9-2010 at 16:02
by: mnick12 |
Anorganic peroxides
I have both barium and strontium peroxide, none of the two are very interesting for energetic purpos ... |
12-9-2010 at 14:31
by: mnick12 |
Opening lithium batteries with copper tube cutters
The bubbles are probably from moisture in your white spirits, nothing to be worried about unless the ... |
11-9-2010 at 10:46
by: mnick12 |
Synthesis of Diisopropyl-ether
Ahhh well you will not get any DIP,
I once was under the same impression as you, that is getting D ... |
11-9-2010 at 10:42
by: mnick12 |
explosive nitrite esters
Mewrox99, the reason why you add a small amount of sulfuric acid or similar acid to an esterificatio ... |
29-8-2010 at 11:04
by: mnick12 |
Thiourea Dioxide --> better than borohydride?
Well I got some vanillin a while ago, and if I have the time tomorrow I will make some more TUD and ... |
28-8-2010 at 22:53
by: mnick12 |
explosive nitrite esters
There tends to be more ester formation if there is some water present in the reactants. |
28-8-2010 at 22:30
by: mnick12 |
Elemental Scientific, LLC
Yes they do take their sweet time,
Since my other post I have made a few other orders, and months l ... |
26-8-2010 at 20:17
by: mnick12 |
Methylxanthine Extraction
What are you planning on extracting theophylline from?
I personally have had trouble extracting an ... |
23-8-2010 at 19:00
by: mnick12 |
Art Chemicals Fraud - Don't waste money at Art Chemicals
Ahhh I almost expected this. I have been looking at their site, and a few things jumped out at me. T ... |
19-8-2010 at 16:00
by: mnick12 |
Ammonium gas from calcium ammonium nitrate fertilizer
I suspect it is due to calium hydroxides insolubility. Try something else like NaOH or KOH or even a ... |
16-8-2010 at 14:54
by: mnick12 |
Extraction of Iodine from Tincture - A Question of Mechanics
Well the HCl would react with KI to give HI and KCl, and the HI would be oxidized to elemental iodin ... |
11-8-2010 at 18:28
by: mnick12 |
good pump?
Nice,
When my pump arrives I will go ahead and post some pics of the ancient beast. Which reminds m ... |
9-8-2010 at 18:34
by: mnick12 |
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