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NITROETHANE: 3 Less Common Procedures
[rquote=270957&tid=17738&author=AndersHoveland][rquote=270949&tid=17738&author=weimi ...
7-1-2013 at 17:39
by: UnintentionalChaos
Pretty Pictures (1)
[rquote=270712&tid=14644&author=CaliusOptimus]DJF90 has got some of the sweetest gear on sci ...
5-1-2013 at 22:25
by: UnintentionalChaos
Alkali metal synthesis
http://www.sciencemadness.org/talk/viewthread.php?tid=6981&page=2

http://www.sciencemadness.o ...
28-12-2012 at 23:06
by: UnintentionalChaos
Synthesis of unsym.-heptachloropropane and hexachloropropene (updated)
I would like to report my successful repetition of the unsymmetrical heptachloropropane procedure. I ...
19-12-2012 at 16:11
by: UnintentionalChaos
No F2 in element webshops : why ?
[rquote=269109&tid=16572&author=99chemicals]Could you theoretically use a CaF2 vial to store ...
18-12-2012 at 18:53
by: UnintentionalChaos
The synthesis of 1 and 2-naphthols from Napththalene
[rquote=268890&tid=11663&author=Magpie]
In reference to the making of Nerolin, do you have ...
16-12-2012 at 14:30
by: UnintentionalChaos
The synthesis of 1 and 2-naphthols from Napththalene
[rquote=268779&tid=11663&author=Magpie][rquote=268775&tid=11663&author=Unintentional ...
16-12-2012 at 10:58
by: UnintentionalChaos
Pretty Pictures (1)
[rquote=268807&tid=14644&author=Pyro]meh, I used a stoich. amount. next time ill add a littl ...
15-12-2012 at 12:07
by: UnintentionalChaos
The synthesis of 1 and 2-naphthols from Napththalene
Nice work, as always, Magpie.

I'll probably be replicating this shortly since 2-ethoxynaphthalene ...
14-12-2012 at 16:48
by: UnintentionalChaos
propanoyl chloride or ?
Propionyl Chloride boils at 77C. Using thionyl chloride, which boils at 75C and produces lots of gas ...
13-12-2012 at 17:14
by: UnintentionalChaos
The most funny mistake I ever saw
The NaBr/KMnO4 mix with sulfuric acid added is my preferred method of making bromine. It generally g ...
8-12-2012 at 16:52
by: UnintentionalChaos
Chlorination of dioxane, what's the mechanism?
This is quite an interesting reaction. Based on the trans geometry, I expect a halonium ion intermed ...
7-12-2012 at 23:23
by: UnintentionalChaos
Very odd reaction
[rquote=267892&tid=22626&author=Poppy]Pardon me for asking to reformulate, not the question ...
6-12-2012 at 16:01
by: UnintentionalChaos
Simple Vanillin Extraction
Find a cheap vanilla extract that contains mostly water, ethanol, and vanillin. Boil off the ethanol ...
6-12-2012 at 13:35
by: UnintentionalChaos
Purifying this store bought ammonia
[rquote=261731&tid=21690&author=unionised]If the cloudy stuff was sodium carbonate, it would ...
3-12-2012 at 21:39
by: UnintentionalChaos
Latest chemical order?
[rquote=267613&tid=9890&author=mr.crow]Yay my expensive ass-caps shipped![/rquote]

[img]h ...
3-12-2012 at 19:42
by: UnintentionalChaos
Nitric acid/silver nitrate stains
Sandpaper?
3-12-2012 at 17:58
by: UnintentionalChaos
Latest chemical order?
[rquote=267401&tid=9890&author=Mailinmypocket]
Aniline! Nice! I'm looking for a source of i ...
1-12-2012 at 01:35
by: UnintentionalChaos
Liquid Fire Drain Cleaner
Liquid fire is fine. It contains a fraction of a percent of alkylpyridine inhibitors, but this does ...
30-11-2012 at 19:18
by: UnintentionalChaos
Nitroethane in DMSO - distill separation?
[rquote=266995&tid=22490&author=chucknorris]DMSO is tricky one since pretty much every solve ...
26-11-2012 at 08:08
by: UnintentionalChaos
BHT Synthesis
[rquote=266958&tid=22484&author=chemrox]Have you tried the unpublished lab procedure? I wou ...
26-11-2012 at 07:53
by: UnintentionalChaos
Oxidation to nitriles...
See also www.sciencemadness.org/talk/files.php?pid=216672&aid=15300
25-11-2012 at 17:24
by: UnintentionalChaos
BHT Synthesis
I feel like this belongs in beginnings...

Has anyone seen a lab scale prep of BHT (2,6-di-tert-bu ...
25-11-2012 at 16:24
by: UnintentionalChaos
Analysis of rocks\minerals without HF
[rquote=266612&tid=22427&author=bfesser]
<li>Mt. St. Helens ash from <a href="http ...
25-11-2012 at 09:45
by: UnintentionalChaos
Making Chlorine
Go read the prepublications forum.

[Edited on 11-25-12 by UnintentionalChaos]
24-11-2012 at 19:21
by: UnintentionalChaos
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