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Qualitative V/Cr detection
[rquote=656952&tid=157212&author=clearly_not_atara]Ammonium metavanadate has a particularly ...
24-3-2021 at 17:42
by: S.C. Wack
Qualitative V/Cr detection
[rquote=656923&tid=157212&author=DraconicAcid]I believe vanadium gives a red colour under th ...
24-3-2021 at 14:36
by: S.C. Wack
Sodium Ethoxide and anhydrous EtOH
[rquote=656750&tid=2656&author=artemov]It's harmless right?[/rquote]

Weigh before and aft ...
21-3-2021 at 12:05
by: S.C. Wack
First o-toluidine synthesis - running into some issues with the reaction mixture
[rquote=656477&tid=157162&author=SuperOxide]Is there an endpoint I can look for?[/rquote]

...
15-3-2021 at 17:23
by: S.C. Wack
First o-toluidine synthesis - running into some issues with the reaction mixture
[rquote=656457&tid=157162&author=Fery]you can find experiments with alternative routes of re ...
15-3-2021 at 16:07
by: S.C. Wack
Anyone else in the US having issues finding OTC sodium bromide?
Perhaps some areas are more into hot tubs than others?

If found at a big box national store it wi ...
11-3-2021 at 18:21
by: S.C. Wack
Prices of Palladium and Rhodium have SKYROCKETED - here's what I see happening.
[rquote=656114&tid=154883&author=Fleaker]More is lost than is recycled.[/rquote]

Recyclin ...
10-3-2021 at 18:54
by: S.C. Wack
What can I make from sodium metasilicate?
Silica gel and florisil. Adsorb something colored on them; now they have color.
10-3-2021 at 18:48
by: S.C. Wack
Speculative investments in chemical elements
Is the melt value of US 1-5 cent pcs. still higher than the cost?
10-3-2021 at 18:45
by: S.C. Wack
Anyone else in the US having issues finding OTC sodium bromide?
[rquote=656107&tid=157140&author=Texium (zts16)]Maybe you were remembering the brominating t ...
10-3-2021 at 18:37
by: S.C. Wack
Beta-Alanine amino acid copper salt
[rquote=656011&tid=157060&author=Bezaleel]Gmelin's doesn't seem to mention anything about th ...
7-3-2021 at 15:52
by: S.C. Wack
Prices of Palladium and Rhodium have SKYROCKETED - here's what I see happening.
Catalyst technology and use shifted to Pd before and esp. after the Soviet stock was [url=https://ww ...
7-3-2021 at 12:03
by: S.C. Wack
Beta-Alanine amino acid copper salt
Gmelin's
7-3-2021 at 11:52
by: S.C. Wack
Mercury pyroantimonate challenge
Yes its the red mercury.
6-3-2021 at 19:36
by: S.C. Wack
What is the difference between flash chromatography and dry chromatography?
[rquote=655922&tid=157126&author=wg48temp9]dry chromatography is packed dry with some compr ...
6-3-2021 at 07:40
by: S.C. Wack
Preparation of Mononitrotoluenes (o-, p-)
[rquote=642812&tid=29111&author=S.C. Wack]The m is in the p.[/rquote]

JCS (Transactions) ...
5-3-2021 at 06:43
by: S.C. Wack
Preparation of Mononitrotoluenes (o-, p-)
Attached here is part of the uncredited reference of COPAE and quite likely also [url=https://www.er ...
3-3-2021 at 16:47
by: S.C. Wack
Preparing CaO from carbonate or hydroxide?
[rquote=644462&tid=156138&author=macckone]Sodium hydroxide as an impurity is an effective fl ...
11-9-2020 at 13:21
by: S.C. Wack
Vanillin bisulfite adduct
Solubility has a lot to do with concentration but it makes no sense to purify a nicely crystalline m ...
11-9-2020 at 13:05
by: S.C. Wack
Preparing CaO from carbonate or hydroxide?
Perhaps in supercritical water it does.

It's funny how the conservative talkers complained about ...
10-9-2020 at 17:17
by: S.C. Wack
Preparing CaO from carbonate or hydroxide?
[rquote=644387&tid=156138&author=macckone]SC Wack,
Someone earlier suggested the hydroxide ...
9-9-2020 at 15:26
by: S.C. Wack
Preparing CaO from carbonate or hydroxide?
The directions I suggested are for use with a fancy contraption known as a lid. At max heat I'd thin ...
8-9-2020 at 18:13
by: S.C. Wack
Preparing CaO from carbonate or hydroxide?
[rquote=644370&tid=156138&author=macckone]550C is the point where the outgassing exceeds nor ...
8-9-2020 at 14:31
by: S.C. Wack
Preparing CaO from carbonate or hydroxide?
It would be nothing to not do this, but it wouldn't take much more effort to do 100 g in a small sau ...
7-9-2020 at 13:11
by: S.C. Wack
Well-known reaction of KMnO4 and HCl: how well-known is it really?
Not so sure chemists of yesteryear (up to 1930 or so referenced by Mellor vol 12 pp 374-380) would a ...
4-9-2020 at 13:47
by: S.C. Wack
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