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Interesting hydrodechlorination of PCE to (edit) dichloroethylene
That is an interesting paper Opylation. I have a synthesis in mind that requires dichloroethylene an ... |
20-6-2021 at 12:58
by: Boffis |
Vicinal dione monoxime in aqueous medium?
I agree with c_not_a that the blue solution is N2O3 in the immiscible layer of butanone which has fo ... |
20-6-2021 at 04:25
by: Boffis |
Derivatising p-dichlorobenzene through its nitro compound
The further nitration of 2-nitro-1,4-dichlorobenzene
This procedure is taken from a paper by Page ... |
19-6-2021 at 10:00
by: Boffis |
Derivatising p-dichlorobenzene through its nitro compound
Hi Fery, do you have any idea of the stoichiometry of the dithionite reduction of nitro compounds? A ... |
19-6-2021 at 08:04
by: Boffis |
Vicinal dione monoxime in aqueous medium?
Hi Karlos, but you used THF as a solvent I am talking about carrying out this reaction in water with ... |
17-6-2021 at 08:08
by: Boffis |
Vicinal dione monoxime in aqueous medium?
In this thread by magpie;
http://www.sciencemadness.org/talk/viewthread.php?tid=8122#pid91211
... |
16-6-2021 at 12:30
by: Boffis |
Nicotinamide dehydration
Hi Pumukli, did you ever try this again with any of the alternative suggestions? |
15-6-2021 at 01:28
by: Boffis |
Benzil dioxime
While searching for other information I stumbled across this short article that gives a procedure fo ... |
9-6-2021 at 00:36
by: Boffis |
Benzil dioxime
Hi Knowledge_seeker, kmno4’s suggestion that the main product may be oxanilide suggests that a Bec ... |
5-6-2021 at 10:19
by: Boffis |
Question about sulfonation of furan
I don't know what your motivation for looking at furan sulphonic acids is but there is another route ... |
3-6-2021 at 07:51
by: Boffis |
Benzil dioxime
Many mono-oximes can exist in two forms if the ketone is asymmetrical. So I guess with two adjacent ... |
29-5-2021 at 22:39
by: Boffis |
Vilsmeier reagent/POCl3 formation
@ mr_bovinejony; Very interesting work, I don't think I've seen an actual V-H synthesis reported on ... |
27-5-2021 at 09:44
by: Boffis |
Aminoguanidine bicarbonate from urea, P2O5, and hydrazine
Cyanamide is only stable in the presence of acetic acid at low temperature ie <20 C. Furthermore ... |
22-5-2021 at 09:07
by: Boffis |
Aminoguanidine bicarbonate from urea, P2O5, and hydrazine
@Uranylperoxysulfate. I wouldn't bother making calcium cyanamide, it is easily bought. I don't know ... |
21-5-2021 at 08:00
by: Boffis |
Azo dye: p-aminophenol and 4-chloro-2-nitrophenol
Hi night429, have you looked at this thread?
http://www.sciencemadness.org/talk/viewthread.php?ti ... |
16-5-2021 at 22:44
by: Boffis |
Azo dye: p-aminophenol and 4-chloro-2-nitrophenol
Hi night429; I have found that it is better to store p-aminophenol as its hydrochloride. It can be o ... |
16-5-2021 at 20:02
by: Boffis |
Drying pseudonitrosites
Nice work dicyanin! I must admit that I have never had need to prepare pseudonitrosites but the abil ... |
13-5-2021 at 09:09
by: Boffis |
Making silicon tetrachloride
Could you use ferrosilicon instead of trying to make magnesium or aluminium silicide. It is easily a ... |
13-5-2021 at 06:07
by: Boffis |
Synthesis of 4-chloro-2-nitrophenol
Hi night429, nice work, its always good to see some practical chemistry being done. The colours refe ... |
11-5-2021 at 07:47
by: Boffis |
synthesis of methyl iodide from methanol, HCl and sodium iodide?
No apology needed for waking the dead! Nice experiment and fairly succesful. The slightly lower yiel ... |
9-5-2021 at 09:31
by: Boffis |
methanol/ionic liquid electroplaing of metals
I don't think methanol is going to work for either group of metals, as you suggest . I think you wil ... |
3-5-2021 at 08:05
by: Boffis |
Capsasin Hydrolysis
Hi Triflic, Since capsaicin dust irritates the eyes like hell you need to protect the whole face. A ... |
2-5-2021 at 09:31
by: Boffis |
Capsasin Hydrolysis
Hi Triflic acid, sorry about my U2U question I hadn't seen this thread then. I think alkali hydrolys ... |
30-4-2021 at 10:55
by: Boffis |
A Note on the Synthesis of 3-Nitrophthalic Acid
After nitrating 31.7 g of phthalic anhydride, I poured the reaction mixture into 90 mL of water, fil ... |
27-4-2021 at 13:13
by: Boffis |
Path to 4-Anisaldehyde
There are many methods of introducing an aldehyde group into an activated aromatics so why not start ... |
27-4-2021 at 06:51
by: Boffis |
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