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oleum & SO3
Today I successfully made some SO3. I dehydrated ~100mL of H3PO4, not at red heat but pretty bloody ...
11-9-2007 at 05:50
by: Antwain
Preparation of cyanides
I looked into the Bucher process before deciding how to try to make cyanide. After looking closely a ...
31-8-2007 at 11:23
by: Antwain
Funny experiment with purple and yellow smoke
Sorry, its been a long time. I have isolated but not dried/ removed nitric acid from several grams o ...
30-8-2007 at 09:05
by: Antwain
Riddle with chromium(III)
As an interesting coincidence i am trying to make several 'chrome alums' myself atm from reduction o ...
30-8-2007 at 08:53
by: Antwain
Funny experiment with purple and yellow smoke
I am going to try to make me some HIO3 today, as soon as the sun comes up in an hour even, and with ...
17-8-2007 at 12:39
by: Antwain
Funny experiment with purple and yellow smoke
I cant be sure that it isn't I3-, I just have a gut feeling that I2 isn't going to form adducts with ...
16-8-2007 at 10:34
by: Antwain
Funny experiment with purple and yellow smoke
Pretty sure thats got absolutely nothing to do with I3-, not being in any kind of solution and all. ...
14-8-2007 at 20:42
by: Antwain
Preparation of cyanides
Well I did it, kind of.

Theoretical reactions;
K4[Fe(CN)6] + 5H2SO4 ----> 4KHSO4 + FeSO4 + 6H ...
12-8-2007 at 01:53
by: Antwain
Seperation of nickel and copper in solution - a practical method.
No doubt there are better ways if you have the right equipment and reagents, which I didn't 5 years ...
12-8-2007 at 00:03
by: Antwain
Seperation of nickel and copper in solution - a practical method.
I decided to post this in case it is of any help to anyone. I have never seen this in literature and ...
11-8-2007 at 04:59
by: Antwain
Preparation of cyanides
actually, a much better antidote is amyl/butyl nitrite, which oxidises hemoglobin to met-hemoglobin ...
8-8-2007 at 00:50
by: Antwain
Simple Americium 241 Experiments?
When I was considering playing with smoke detectors (I recall that you would get a visible yield, ba ...
6-8-2007 at 15:38
by: Antwain
Preparation of cyanides
And a word of warning (this was a pretty stupid mistake) :(

DON'T put alkaline solutions in PET b ...
6-8-2007 at 15:17
by: Antwain
Preparation of cyanides
kmo4, could you describe briefly the procedure you used, especially with regard to heating method (w ...
3-8-2007 at 17:37
by: Antwain
Preparation of cyanides
Yeah, cyanide is the most poisonous thing I have ever attempted. But safety first - the minimum quot ...
31-7-2007 at 08:19
by: Antwain
Preparation of cyanides
Hi all.

This is my first post of what will hopefully be many. I have always been fascinated by cy ...
28-7-2007 at 11:33
by: Antwain

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