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Microscale Prep of Anhydrous Alcl3
Thought this might be useful as it makes a difficult reagent easy to get.
[file]11007[/file] |
26-7-2010 at 03:26
by: rrkss |
Anhydrous Alcl3
... ,
I Was just wondering if anybody had any idea's as to the cheapest way to manufacture Anhydrous Alcl3 for use in Friedel-Crafts
reactions. I Know that you can bubble chlorine gas through molten Al ... |
10-8-2009 at 22:47
by: SunlightChemist |
Easy anhydrous Alcl3 production
... g about recently. I have spent alot of tie trying to produce 100 gram scale quantities of anhydrous Alcl3. I have experimented with Al
powder is a variety of solvents, with dry HCL gas bubbled throug ... |
21-7-2009 at 11:13
by: greenimp |
Alcl3 Anhydrous
Have in stock, Alcl3 Anhydrous reagent grade.
25g, 100g amounts.
$16.00 for 25g
$35.00 for 100g
Pantry Scient ... |
16-4-2009 at 00:40
by: undead_alchemist |
A new demethylation reagent pair: Alcl3/Thiourea
... tml[/url]
Here is what what was said to have worked for vanillin.
"A solution of 212g (1.6 M) Alcl3 (anhydrous) and 63.28g (0.8 M) Thiourea in 1L of DCM was made and let stir for 30 mins at room ... |
20-12-2008 at 16:10
by: greenimp |
nitromethane co-ordination of Alcl3
[quote]Actually, according to Kinetic, Alcl3 can be used in the Friedel-Crafts reaction of benzodioxole with Et-COCl if nitromethane is
use ... |
29-9-2007 at 05:39
by: Epopteia |
Anhydrous Alcl3??
Hey everyone.
I want to make anhydrous aluminum chloride to use as a catalyst in a reaction i am wo ... |
10-9-2006 at 16:10
by: sonogashira |
recrystallization of Alcl3.6H2O
[How can i prepare the hexa hydrated aluminium chloride from it's solution ? reply soon.i am confus ... |
30-12-2005 at 03:47
by: govinda |
HCl and Al, Alcl3?
... etely (additional Al causes little to no reaction) litmus is red in solution.
6HCl + 2Al --> 2Alcl3 + 3H2
is what I've come up with.
Questions. Does the solution I have contain Alcl3? ... |
15-2-2004 at 23:06
by: thunderfvck |
purification of Alcl3
yes, I just checked Mercks Chemdat.
Alcl3 sublimes at 181 deg C, and decomposes (into what?) at 262 deg C.
However there is a better ... |
4-9-2003 at 14:57
by: chemoleo |
