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making sodium ethyl sulfate from spent acid-ether reaction mixture On your last point, I wonder if cautiously adding H2O2 to the spent reaction acid mixture could rege ...	25-9-2024 at 22:55 by: jackchem2001
Diethylether (sulfuric acid saving method) The ethylene byproduct and low conversion per pass with alumina is a bit unfortunate. Having multipl ...	25-9-2024 at 19:56 by: jackchem2001
Diethylether (sulfuric acid saving method) I realized my original post doesn't make this very clear but I am bubbling the ethanol into the mixt ...	21-9-2024 at 19:42 by: jackchem2001
Diethylether (sulfuric acid saving method) I think I may have found a way to improve the typical lab scale ether preparation. Usually, liquid e ...	20-9-2024 at 22:39 by: jackchem2001
DIY water aspirator vacuum pump The vacuum is limited by the vapor pressure of the fluid, so a low vapor pressure oil would be ideal ...	11-9-2024 at 17:28 by: jackchem2001
Isolation of Chloral Hydrate In the presence of water, the aldehyde will form a diol which is further oxidized to the carboxylic ...	11-9-2024 at 17:26 by: jackchem2001
DIY water aspirator vacuum pump How are you determining your level of vacuum?	8-9-2024 at 03:54 by: jackchem2001
Amateur Friendly Aliphatic Aldehyde Reduction I was under the impression that Pd/C (and other metals) catalyzed hydrogenation generally do not red ...	7-9-2024 at 20:23 by: jackchem2001
Diethylether (sulfuric acid saving method) [rquote=695169&tid=160329&author=MrDoctor] testing ether % with cold calcium chloride solut ...	6-9-2024 at 18:06 by: jackchem2001
"Let's Distill Some H2SO4!" -Last Words [rquote=694891&tid=160300&author=metalresearcher]What I miss in this topic is that why TO do ...	25-8-2024 at 19:45 by: jackchem2001
Suggestions on vacuum pump purchase I found that when measuring the vacuum pressure with a gauge, I had to coat the thread in silicone g ...	14-8-2024 at 22:08 by: jackchem2001
Off-topic conjecture split from "A foray into phenethylamines of the Shulgin kind" Phenyl esters have anhydride-like pi character and so are not very stable. At some point I want to t ...	14-8-2024 at 22:03 by: jackchem2001
"Let's Distill Some H2SO4!" -Last Words I have not done this hazardous procedure so these are just my speculations on some of the posts in t ...	9-8-2024 at 19:44 by: jackchem2001
Ethylchloride preparation From https://www.orgsyn.org/demo.aspx?prep=CV2P0279, this may work with NaCl and ethanol instead ...	5-8-2024 at 19:49 by: jackchem2001
Acrylic acid by dehydration of Lactic acid? I don't have much to contribute but from the structure of lactic acid I think a carbon monoxide dete ...	4-8-2024 at 15:09 by: jackchem2001
Preparation of ionic nitrites An oxidizing agent is one which can accept a lone pair and eliminate an adjacent proton. Nitric acid ...	19-7-2024 at 21:14 by: jackchem2001
Preparation of ionic nitrites Thanks for all of the comments [rquote=694147&tid=52&author=Sir_Gawain]I’ve also had a ...	16-7-2024 at 17:54 by: jackchem2001
Preparation of ionic nitrites I have attempted reduction of KNO3 with CaSO3 a couple of times. I will leave some observations here ...	11-7-2024 at 04:54 by: jackchem2001
Diethylether (sulfuric acid saving method) Continuing from my last post suggesting the addition of sodium sulfate to catalyse the formation of ...	3-7-2024 at 01:04 by: jackchem2001
Homemade and Repurposed Lab Gear It is common to use aluminium foil to create an insulating layer of air around a boiling flask. If t ...	24-6-2024 at 21:21 by: jackchem2001
Diethylether (sulfuric acid saving method) After experimenting with this procedure a little bit I would like to put something into text that is ...	13-6-2024 at 07:19 by: jackchem2001
The Short Questions Thread (4) A base bath is said to clean glassware by etching a small layer off the glass. How does this affect ...	11-6-2024 at 19:57 by: jackchem2001
Pyrazinoate from 2-acetylpyrazine The point is the reactivity of the planar nitrogens in the ring [quote]The reaction mixture turne ...	4-6-2024 at 06:32 by: jackchem2001
Pyrazinoate from 2-acetylpyrazine [quote]My first step would need to be to get rid of that methyl ketone by oxidizing it into a carbox ...	3-6-2024 at 21:46 by: jackchem2001
The Short Questions Thread (4) When using tight steel hose clamps, is there a risk of implosion under vacuum? [img]https://i.img ...	3-6-2024 at 02:32 by: jackchem2001
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