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Acetic anhydride preparation
@paulll, yes, stoichiometrically the yields from phosphorus pentoxide reagent are terrible haha. I ... |
27-5-2024 at 08:51
by: greenlight |
Acetic anhydride preparation
Thankyou for the replies,
Would it be possible to run the reaction by slowly dripping glacial acet ... |
26-5-2024 at 09:58
by: greenlight |
Acetic anhydride preparation
Has anyone on here had any success with the reaction of phosphorus pentoxide and glacial acetic acid ... |
22-5-2024 at 10:11
by: greenlight |
Life after detonation
The right hand came out brilliantly compared to the first photo.
I always remember your accident ... |
19-5-2024 at 10:17
by: greenlight |
Pretty Pictures (2)
Some Cesium nitrate precipitating crystals out of solution as the water evaporates slowly.
[Edited ... |
8-2-2024 at 04:01
by: greenlight |
Concentrating Sulfuric Acid through Boiling
If you have a pure solution of sulfuric acid in water at a low concentration then there are two obse ... |
5-12-2023 at 02:57
by: greenlight |
Short question / quick answer - Thread
How have you stored the polyisobutylene? Away from heat, moisture and direct sunlight?
The only thi ... |
1-12-2023 at 06:09
by: greenlight |
Using a vacuum filtration flask in vacuum distillation?
[rquote=685545&tid=159668&author=Texium] I wouldn’t consider IKA to be reliable. Their dev ... |
11-7-2023 at 18:27
by: greenlight |
Using a vacuum filtration flask in vacuum distillation?
If your looking reasonably priced there is plenty of cheap chinese models on ebay but these can be p ... |
10-7-2023 at 01:36
by: greenlight |
Cocrystalization
"I dunno if cocrystalized liquids with solids like EGDN and PETN after cocrystalization the evapora ... |
7-7-2023 at 11:21
by: greenlight |
Cocrystalization
It seems there is a larger proportion of CL-20 to HMX is the usual ratio to create the cocrystal str ... |
6-7-2023 at 20:14
by: greenlight |
Chemistry behind RDX
[rquote=680432&tid=150602&author=ManyInterests]On second thought (I cannot edit my message f ... |
16-1-2023 at 10:46
by: greenlight |
Chemistry behind RDX
[rquote=680405&tid=150602&author=ManyInterests]I didn't stir, maybe I should have, but I thi ... |
16-1-2023 at 10:29
by: greenlight |
Chemistry behind RDX
[rquote=680288&tid=150602&author=ManyInterests]My gas wash bottle is quite small, so I will ... |
12-1-2023 at 12:14
by: greenlight |
Pretty Pictures (2)
[rquote=680246&tid=26378&author=arkoma]First go at Picric Acid.
[/rquote]
Beauti ... |
10-1-2023 at 10:52
by: greenlight |
Chemistry behind RDX
[rquote=680250&tid=150602&author=ManyInterests][quote]
A better method to WFNA is by bubbli ... |
10-1-2023 at 10:43
by: greenlight |
Chemistry behind RDX
[rquote=680243&tid=150602&author=Herr Haber]The blue caps are just PP so it's not surprising ... |
10-1-2023 at 10:38
by: greenlight |
Chemistry behind RDX
[rquote=680217&tid=150602&author=ManyInterests]So ammonium nitrate then.
At any rate, I a ... |
9-1-2023 at 10:35
by: greenlight |
Chemistry behind RDX
[rquote=678371&tid=150602&author=ShotBored][rquote=678090&tid=150602&author=greenlig ... |
9-1-2023 at 10:19
by: greenlight |
Chemistry behind RDX
I have made RDX a few times and from searching around here, these are the only details I could find: ... |
1-11-2022 at 08:57
by: greenlight |
Countertop dishwasher for cleaning lab glassware?
One thing I have noticed from using a dishwasher years ago for beakers is that if you use the small ... |
15-7-2022 at 10:25
by: greenlight |
Are hotplate stirrers unreliable?
I wouldn't say they are unreliable. I have never brought Chinese hotplate/stirrers though. Only a ... |
15-7-2022 at 10:17
by: greenlight |
Heating mantle smoking
Had the same experience with a new chinese heating mantle. Was seriously worried there was a wiring ... |
15-7-2022 at 10:07
by: greenlight |
Strange synthesis of UN?
I am aware of this method as I did the exact thing you describe with hardware store urea and 62% nit ... |
14-4-2022 at 09:03
by: greenlight |
New Energetic Materials - Current Research
Full-nitro-nitroamino cooperative action: Climbing the energy peak of benzenes with enhanced chemica ... |
29-3-2022 at 00:34
by: greenlight |
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