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Exotic Primaries - Complex Salts
Both exist as solids at STP, but Semicarbazide is likely just too hygroscopic and basic, so it’d f ...
9-6-2024 at 16:55
by: dettoo456
Exotic Primaries - Complex Salts
Chemically, Semicarbazide is more stable. The hydrazine bond is less stable than the simple amide. B ...
9-6-2024 at 11:29
by: dettoo456
I have 5% Pd/C and need a reaction to do...
Pretty much all Pd/C is used for is hydrogenations. If you don’t have the equipment or reagents th ...
8-6-2024 at 19:51
by: dettoo456
Exotic Primaries - Complex Salts
Carbohydrazide (1,3-diaminourea) can be prepared by amination of Semicarbazide with Hydrazine or jus ...
6-6-2024 at 19:09
by: dettoo456
Trifluoroacetic anhydride?
Yea, preparing acetic anhydride (or any anhydrous acid at that) is a headache in its own right, not ...
4-6-2024 at 05:37
by: dettoo456
5-ATZ(5-Aminotetrazole), the nitrotetrazolate ion and friends
Oh, the diazoaminotetrazole actually thermally rearranges to Tetrazene in the reaction with acetic a ...
3-6-2024 at 07:13
by: dettoo456
5-ATZ(5-Aminotetrazole), the nitrotetrazolate ion and friends
I’m not sure what the diazoaminotetrazole you speak of is. But the Cu(ii)-5,5’-azobis(tetrazolat ...
1-6-2024 at 12:09
by: dettoo456
Pentaerythritol (mono) for sale - US
I have 20kgs of monoPentaerythritol available (as a dry, granular powder). If anyone is interested, ...
28-5-2024 at 16:29
by: dettoo456
Short question / quick answer - Thread
Has anyone carried out a destructive nitration procedure on a ketone before? I couldn’t find much ...
28-5-2024 at 08:08
by: dettoo456
Exotic Primaries - Complex Salts
Melamine itself has solubility issues in water, so a salt would be needed, and I don’t know how pr ...
25-5-2024 at 19:24
by: dettoo456
Hard to find, high quality reagents and glassware for sale!
Goes without saying, but Texium ships fast, is extremely helpful and fair with items and pricing, an ...
25-5-2024 at 19:17
by: dettoo456
Acetic anhydride preparation
If someone needs the Ac2O for a simple friedel crafts (or some other carboxylic anhydride for that p ...
23-5-2024 at 06:27
by: dettoo456
5-ATZ(5-Aminotetrazole), the nitrotetrazolate ion and friends
The nitrous acid won’t decompose very fast if you carry out the procedure at a normal pace at the ...
23-5-2024 at 05:54
by: dettoo456
5-ATZ(5-Aminotetrazole), the nitrotetrazolate ion and friends
NaNTz seems to be very soluble in Acetone and 5ATz only moderately so. But, the actual nitrosation o ...
22-5-2024 at 05:46
by: dettoo456
Short question / quick answer - Thread
Didn’t read it fully, but this may help:



[Edited on 20-5-2024 by dettoo456]
20-5-2024 at 09:00
by: dettoo456
Short question / quick answer - Thread
Has anyone noticed some papers describing odd synthesis methods for EMs? The paper linked below desc ...
15-5-2024 at 07:39
by: dettoo456
High MW PIB (Oppanol N150) for sale
Selling some Oppanol N150 (BASF’s highest MW PIB) in 250g amounts (big chunks of it in a bag). I h ...
12-5-2024 at 12:32
by: dettoo456
Short question / quick answer - Thread
Although there doesn’t seem to be much info on it, the detonation velocity (from the few sources I ...
9-5-2024 at 07:13
by: dettoo456
Processing of plastisol compositions
I am not sure about the compositions you mentioned, but I know for lots of plastics, the active EM c ...
7-5-2024 at 09:47
by: dettoo456
Most Cost-Effective Explosive
[rquote=692899&tid=160313&author=4-Stroke]Hello everyone! Although I have lurked here for qu ...
6-5-2024 at 09:00
by: dettoo456
New ETN Synthesis
Crashing the nitration mixture into a Urea sol is pointless and wasteful, as the mixed acids could p ...
1-5-2024 at 17:27
by: dettoo456
Short question / quick answer - Thread
DCM will dissolve nitric acid very readily, though I don’t know how soluble the hydantoin is in DC ...
1-5-2024 at 17:20
by: dettoo456
Short question / quick answer - Thread
Mononitration at the 1 position likely wouldn’t be too difficult but the dinitration would definit ...
30-4-2024 at 07:47
by: dettoo456
3-aminopropionitrile fumurate
Propionitrile itself is exceedingly toxic just by itself, so no wonder this analogue might be hard t ...
22-4-2024 at 07:02
by: dettoo456
Det Cap Strategies
https://apps.dtic.mil/sti/pdfs/AD1063959.pdf

https://ndiastorage.blob.core.usgovcloudapi.net/ndia ...
19-4-2024 at 05:44
by: dettoo456
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