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Setting up a burner Sorry for bringing up an old thread.
I have a teclu burner, which I belive is designed to work on ... |
22-4-2011 at 07:01 by: Zinc |
Hydrazine [rquote=204312&tid=1128&author=NurdRage]thats actually really good considering low concentra ... |
15-3-2011 at 08:05 by: Zinc |
Hydrazine Actualy I failed in my calculations, I calculated how much pure hydrazine should I get, not how much ... |
15-3-2011 at 06:23 by: Zinc |
Hydrazine Fail, if I calculated it correctly that would be cca. 160% yield (based on NaOCl), impossible.
I am ... |
14-3-2011 at 15:55 by: Zinc |
Hydrazine Yesterday I weighed the hydrazine sulphate, and there is 18 g, much more than expected It seems t ... |
14-3-2011 at 06:15 by: Zinc |
Hydrazine I tested the mixture of batches, and indeed there was ketazine in it. I devided it into three portio ... |
11-3-2011 at 07:55 by: Zinc |
Hydrazine Yesterday I made a batch with 17 ml of NH3, 7 ml of MEK and 26 g of NaOCl soln. and let it stay over ... |
11-3-2011 at 03:43 by: Zinc |
Hydrazine The last time I waited around 1-1.5 h, the mix was clear, no turbidity like it would be expected fro ... |
10-3-2011 at 10:40 by: Zinc |
Hydrazine I did antoher try, this time with 15 ml 25% NH3, 6 ml MEK and 24 ml NaOCl, and let the NH3 and MEK r ... |
10-3-2011 at 09:12 by: Zinc |
Hydrazine Today I tried the procedure again but with much smaller quantities.
I used 30 ml of 25% NH3, 12 m ... |
10-3-2011 at 03:00 by: Zinc |
Hydrazine Indeed I added the hypochlorite cca. 1-2 min after the MEK.
I have a question about stirring. Is ... |
8-3-2011 at 15:13 by: Zinc |
Hydrazine Today I tried to make hydrazine sulfate following Nurdrages ketazine process.
The differences wer ... |
8-3-2011 at 11:29 by: Zinc |
KNO3,P, charcoal mixture Be careful when using any mixture containing P, they tend do be very sensitive. |
28-2-2011 at 05:04 by: Zinc |
NO2 ventilation in HNO3 distillation Today I tried to distill HNO3 from a distillation flask closed by a plastic cork (I don't know what ... |
26-2-2011 at 10:45 by: Zinc |
NO2 ventilation in HNO3 distillation I will soon get a 250ml distillation flask, but it doesn't have a ground glass neck so I can't close ... |
19-2-2011 at 06:21 by: Zinc |
Pressed Cast Explosivies? I belive that the ANNM is more "powerfull" than KNO3/NM as AN is itself an explosive, and all the de ... |
2-2-2011 at 14:15 by: Zinc |
Diving Into the World of Fulminates Yesterday I made some Hg(ONC)2.
To cca. 6g of Hg i added 45ml of 60-70% nitric acid (which was ma ... |
2-2-2011 at 06:10 by: Zinc |
Diving Into the World of Fulminates Sorry to bring up an old thread, but this one seemed the most suitable for the question that I have. ... |
27-1-2011 at 11:17 by: Zinc |
nitroglycerin Yesterday I tried to set off a mix of 40g DNT, 30g NG and 5g paint-grade Al powder and cca. 1g of Na ... |
24-1-2011 at 03:24 by: Zinc |
nitroglycerin Sorry for the double post, and if the question is too "practical".
I was thinking about trying NG ... |
21-1-2011 at 11:04 by: Zinc |
nitroglycerin I washed the NG with an another portion of conc. NaCl soln. and transported it with a syringe into a ... |
16-1-2011 at 12:05 by: Zinc |
nitroglycerin My NG has now been 4 days under the NaCl solution. Already after the first day it almost completely ... |
16-1-2011 at 05:37 by: Zinc |
nitroglycerin [rquote=198254&tid=949&author=hissingnoise]
What lack of equipment could possibly prevent y ... |
12-1-2011 at 08:36 by: Zinc |
NG neutralization I have noticed NG can be difficult to properly neutralize.
Two times have I put NG under a NaHCO ... |
12-1-2011 at 05:47 by: Zinc |
Trinitrotoluene preparation Sorry to bring up an old thread, but I didn't want to start a new one.
I tried to make nitrotolue ... |
28-12-2010 at 04:02 by: Zinc |
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