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Liquid primaries
As dettoo says, the lack of voids in a liquid energetic, makes ddt very inefficient. That means that ... |
26-6-2024 at 23:43
by: Microtek |
5-ATZ(5-Aminotetrazole), the nitrotetrazolate ion and friends
No, I haven't tried that. The reason I used the amino substituted triazole specifically, is that I h ... |
26-6-2024 at 23:35
by: Microtek |
Det cap questions: e-match nichrome, selecting a primary
Firearms primer mixture is much more sensitive than a quality primary such as many of the metal amin ... |
18-6-2024 at 23:11
by: Microtek |
PETN recrystallisation procedure for LOW density
@Etanol: My PETN does not contain the impurities you mention, possibly because I synthesize it from ... |
13-6-2024 at 01:37
by: Microtek |
PETN recrystallisation procedure for LOW density
You could do both. First a slow crystallization for obtaining a pure product, then redissolve in fre ... |
9-6-2024 at 01:41
by: Microtek |
PETN recrystallisation procedure for LOW density
The function of urea in this context is not to act as a base, but as a NOx scavenger. The same react ... |
7-6-2024 at 07:53
by: Microtek |
Nickel aminoguanidine diperchlorate
During the usual synthesis of NAP, the solution is boiled for about 5 minnutes. This would drive off ... |
3-6-2024 at 00:04
by: Microtek |
NHN synthesis not working
@ManyInterests: I encourage you to find a copy of the book "Small scale synthesis of Laboratory Reag ... |
11-5-2024 at 07:46
by: Microtek |
Exotic Primaries - Complex Salts
I tried copper, cobalt, zink, iron(III), nickel, aluminum and magnesium as the central ion in 4-amin ... |
2-5-2024 at 22:54
by: Microtek |
Exotic Primaries - Complex Salts
As I commented in another thread, there definitely is a Ni complex with aminoTRIazole, so I find it ... |
1-5-2024 at 12:33
by: Microtek |
5-ATZ(5-Aminotetrazole), the nitrotetrazolate ion and friends
I have recently experimented with 4-amino-1,2,4-triazole as a ligand for nickel perchlorate. I think ... |
21-4-2024 at 09:38
by: Microtek |
Nickel aminoguanidine diperchlorate
[quote]
Chrystal long needle’s sensitivity[/quote]
If you stir it continually during precipi ... |
14-4-2024 at 22:34
by: Microtek |
Nickel aminoguanidine diperchlorate
I would be wary of using ammonia for adjusting pH. I think you risk substituting some of the aminogu ... |
13-4-2024 at 14:00
by: Microtek |
Exotic Primaries - Complex Salts
I don't know how labile the hydrazine ligands are, but I would expect at least some of them to be re ... |
2-4-2024 at 23:43
by: Microtek |
Det Cap Strategies
Yes, I was talking about experiments with caps or similar sizes. The thing with HEs is that they als ... |
1-3-2024 at 00:30
by: Microtek |
Det Cap Strategies
Indeed, the sawdust bucket is an excellent way to iron out any problems with the caps before using t ... |
29-2-2024 at 08:54
by: Microtek |
Det Cap Strategies
I think you should abandon the idea of melt casting the base charge for now. It is possible that it ... |
29-2-2024 at 02:09
by: Microtek |
Det Cap Strategies
I suggest that you do a simple non-experimental cap first. Something like 1 g of pressed ETN or RDX, ... |
26-2-2024 at 23:30
by: Microtek |
Det Cap Strategies
If the caps detonate fully, it won't matter what it is resting on. Like shooting an apple hanging on ... |
25-2-2024 at 23:44
by: Microtek |
5-ATZ(5-Aminotetrazole), the nitrotetrazolate ion and friends
I would think it likely that AgNTz dissolves in ammonia water, forming the soluble diammine silver c ... |
10-2-2024 at 06:15
by: Microtek |
Azides
You should prepare a sample of AgN3 by the regular process (AgNO3 and NaN3 solutions, dropwise addit ... |
9-2-2024 at 03:34
by: Microtek |
Cast vs Plastic
Also, remember that the dimensions and containment of the charge matters greatly, as alluded to abov ... |
3-2-2024 at 03:21
by: Microtek |
NIHT/NHHT Synth Suxess!
Precipitating the free base with NaOH might be a good idea, I'll try that at some point.
I did co ... |
22-1-2024 at 03:27
by: Microtek |
NIHT/NHHT Synth Suxess!
I'm sure that a lot of the crude material was in fact NIHT*HCl. I would say that NIHT is probably a ... |
21-1-2024 at 23:21
by: Microtek |
NIHT/NHHT Synth Suxess!
I gave NIHT a shot recently:
Hexamine (3.5 g, 25 mmol) was added to hydrochloric acid (37%, 10 ml ... |
21-1-2024 at 06:44
by: Microtek |
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