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Cell for smallscale electroreduction of nitroalkenes
After playing for a while with this kind of reduction Tyvex seems to be the best variant as cell div ...
3-9-2017 at 08:22
by: HollowMan
DMT via tryptamine and NaBH4
And Tetrahedron original paper says -15°C instead of 15°C. Isn´t NaBH4 reacting much to slow at - ...
9-8-2017 at 14:46
by: HollowMan
Dimethylation of tryptamine via formaldehyde/STAB
Someone tried Tetrahedron´s method?

(Patent of making Rizatriptan)
18-7-2017 at 05:25
by: HollowMan
DMT via tryptamine and NaBH4
@ Crowfjord

Where did you found this files?

Sth what is missing in the procedure is the actual ...
18-7-2017 at 05:22
by: HollowMan
Experimental: Alternative to Al/Hg - the Al/Cu
Did someone tried the Al/Cu reduction once again successfully with a nitropropene as starting materi ...
4-7-2017 at 04:14
by: HollowMan
DMT via tryptamine and NaBH4
Hi,

I just found this interesting method for synthesis DMT by using tryptamine and NaBH4 as a sta ...
24-6-2017 at 17:53
by: HollowMan
N,N-Dimethylamphetamine byproduct
[rquote=486315&tid=74998&author=UC235]People use shitty impure methylamine made from hexamin ...
24-6-2017 at 17:46
by: HollowMan
N,N-Dimethylamphetamine byproduct
Hello,

I just read some articles on erowid about the illicit synthesis of amphetamine/methampheta ...
24-6-2017 at 07:11
by: HollowMan
Cell for smallscale electroreduction of nitroalkenes
[rquote=479075&tid=4145&author=S.C. Wack][rquote=478870&tid=4145&author=HollowMan]
...
27-3-2017 at 15:03
by: HollowMan
Cell for smallscale electroreduction of nitroalkenes
Alright I´ll tell you how I´ll go on:

First I try the easiest version: Getting a pice of Gorete ...
27-3-2017 at 14:59
by: HollowMan
Cell for smallscale electroreduction of nitroalkenes
I´m not sure how much the resistance deepens on the wall thickness. The condom was so thin but the ...
27-3-2017 at 10:37
by: HollowMan
Cell for smallscale electroreduction of nitroalkenes
[rquote=478999&tid=4145&author=Melgar][rquote=478847&tid=4145&author=HollowMan]I hav ...
27-3-2017 at 00:23
by: HollowMan
Gore-Tex as a cell membrane
[rquote=478954&tid=30448&author=Tsjerk]For me it seemed to work, nice conductivity and as fa ...
26-3-2017 at 10:59
by: HollowMan
Gore-Tex as a cell membrane
Hm so none of you tried an electrochemical reduction with the Goretex membrane?

Would be great i ...
26-3-2017 at 09:30
by: HollowMan
Gore-Tex as a cell membrane
Has anyone tried a successful electrochemical reduction with the Goretex membrane? (as cell divider) ...
25-3-2017 at 18:21
by: HollowMan
Cell for smallscale electroreduction of nitroalkenes
[rquote=478799&tid=4145&author=Corrosive Joeseph]I read somewhere Tyvek material works as we ...
25-3-2017 at 06:09
by: HollowMan
Cell for smallscale electroreduction of nitroalkenes
[rquote=478793&tid=4145&author=Melgar][rquote=478539&tid=4145&author=HollowMan]Hi,
...
25-3-2017 at 01:23
by: HollowMan
Cell for smallscale electroreduction of nitroalkenes
Hi,

I have a view questions about the battery bag method:

- is there any possibility to stick/ ...
22-3-2017 at 07:34
by: HollowMan
L-tryptophan decarboxylation
So thanks a lot for your advices now it´s time for the experimental part. After I will come back an ...
20-9-2015 at 03:57
by: HollowMan
L-tryptophan decarboxylation
1.Did you use just paraffin oil or mixed with DMSO like in hyperlab? They mixed xylene with DMSO and ...
19-9-2015 at 18:33
by: HollowMan
L-tryptophan decarboxylation
Thanks for your extensively reply. At first I thought, this procedure should be the easiest I will e ...
19-9-2015 at 11:34
by: HollowMan
L-tryptophan decarboxylation
I´m 99% sure that is just tryptophan without sth else. Thats whats on the package and on their webs ...
19-9-2015 at 10:22
by: HollowMan
L-tryptophan decarboxylation
Hm ok alright so it´s not sure what will happend during refilxing in DMF.. I don´t have the possib ...
19-9-2015 at 07:39
by: HollowMan
L-tryptophan decarboxylation
I wanted to add, that my tryptophan was sold as a supplement (bulk powders).
Most of the introducti ...
19-9-2015 at 05:13
by: HollowMan
L-tryptophan decarboxylation
Hi,
Of course DMF is no keton but it has the same functional group. Thas what i meant.
Of course ...
19-9-2015 at 04:56
by: HollowMan
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