| Search |
| [Next Page] |
Hitachi D-7000 HPLC Issues
Hi everyone,
Just acquired a Hitachi HPLC from the university trash. I have the interface, the pu ... |
12-11-2018 at 15:24
by: ScienceHideout |
Anyone have experience with Thermolyne Nuova II hot plate stirrer?
I gotta say, I had a Thermolyne Nuova for many years and it served me well until I got a hold of a F ... |
20-10-2018 at 15:04
by: ScienceHideout |
IBM RXN for Chemistry
I think it does have a lot of potential... it can only get better over the years. It would be neat t ... |
1-9-2018 at 07:37
by: ScienceHideout |
IBM RXN for Chemistry
Hi guys,
I know I have been lurking a long time but I have been busy finishing up school as well ... |
31-8-2018 at 04:42
by: ScienceHideout |
Preparation of Succinic Acid
Magpie- Have you tried doing different 'types' of hydrogenations with your catalyst to test it? Such ... |
16-10-2016 at 16:07
by: ScienceHideout |
Preparation of Succinic Acid
[rquote=463239&tid=69635&author=Magpie] I reported the results of my "activity" testing with ... |
16-10-2016 at 12:14
by: ScienceHideout |
Preparation of Succinic Acid
Good writeup, Magpie! I regret that I didn't see it earlier.
I have been working full time lately ... |
8-10-2016 at 17:04
by: ScienceHideout |
How bad does Indole smell?
I have no problem admitting that I like the smell of indole. Everyone I work with thinks it smells b ... |
10-5-2016 at 13:58
by: ScienceHideout |
Green Synthesis of 3-methyl-heptan-3-ol from common materials
Thanks, I will take a look at this more during my free time.
As far as bromide, I suppose one thi ... |
5-4-2016 at 17:40
by: ScienceHideout |
Rotavap operational concern....
I don't know much about fixing rotovaps but I will tell you that the black screwy-thingie with the m ... |
5-4-2016 at 17:35
by: ScienceHideout |
How do you store your chemcials?
To learn about the storage groups and compatible families, type in "Flinn Scientific Chemical Storag ... |
3-4-2016 at 12:50
by: ScienceHideout |
Green Synthesis of 3-methyl-heptan-3-ol from common materials
So I was busy cleaning the lab this morning after all my hard work. I think that my BuBr yield is mo ... |
3-4-2016 at 09:02
by: ScienceHideout |
Green Synthesis of 3-methyl-heptan-3-ol from common materials
gdflp- Interesting facts with the diol, It probably is partially because of the volatility, but I wo ... |
2-4-2016 at 19:51
by: ScienceHideout |
Green Synthesis of 3-methyl-heptan-3-ol from common materials
Great news guys!!!
I was up until 12 last night in the lab refluxing and distilling, and I woke u ... |
2-4-2016 at 09:52
by: ScienceHideout |
Green Synthesis of 3-methyl-heptan-3-ol from common materials
Thanks for the literature, Magpie!
Unfortunately the TCT/DMF prep is not practical for me, becaus ... |
31-3-2016 at 10:14
by: ScienceHideout |
Green Synthesis of 3-methyl-heptan-3-ol from common materials
Hi guys,
DJ, just want to thank you again for all of the criticism, it is appreciated and I will ... |
30-3-2016 at 18:32
by: ScienceHideout |
Green Synthesis of 3-methyl-heptan-3-ol from common materials
DJF90, you outdid yourself! 
Your criticism was very valuable, and you definitely clarified a l ... |
29-3-2016 at 16:52
by: ScienceHideout |
Green Synthesis of 3-methyl-heptan-3-ol from common materials
Magpie, thanks for your input!
I am going to try again this weekend with both parts... I think th ... |
29-3-2016 at 15:41
by: ScienceHideout |
Green Synthesis of 3-methyl-heptan-3-ol from common materials
CuReUs,
Thanks for the suggestion. At this time I don't have any methyl THF, but perhaps I could ... |
29-3-2016 at 08:35
by: ScienceHideout |
Final Draft?
HeYBrO and BromicAcid,
I took your advice and made the following changes.
[list=1][*]I specifi ... |
28-3-2016 at 17:04
by: ScienceHideout |
Are there any practical methods to break an ethanol:heptane azeotrope in the home lab?
Couldn't you add water and do a simple extraction? Hexane is VERY nonpolar, and water is VERY polar. ... |
25-3-2016 at 19:26
by: ScienceHideout |
pipettes
[rquote=442513&tid=65657&author=aga]
What is the definition ?
[/rquote]
[b][u][size ... |
19-3-2016 at 16:28
by: ScienceHideout |
pipettes
I LOVE using pipettes in all of my chemistry experiments. I have a good variety:
Beral pipettes a ... |
19-3-2016 at 13:59
by: ScienceHideout |
Green Synthesis of 3-methyl-heptan-3-ol from common materials
[rquote=440216&tid=65439&author=j_sum1]I am no expert on this so someone else will have to c ... |
27-2-2016 at 20:19
by: ScienceHideout |
Synthesis of longer chain tertiary alcohols
Everyone,
Today I successfully ran a Grignard to make 3-methyl-heptan-3-ol. Please see it in prep ... |
27-2-2016 at 19:39
by: ScienceHideout |
| [Next Page] |
