Sciencemadness Discussion Board
Not logged in [Login ]
Go To Bottom

Printable Version  
Author: Subject: radical-bromination of RDX
BASF
Hazard to Others
***




Posts: 282
Registered: 5-11-2002
Member Is Offline

Mood: hydrophilic

[*] posted on 26-8-2003 at 05:23
radical-bromination of RDX


I´d like to try this next we, i have an idea on how to do it, but its fairly vague.

These are the limits of my equipment:

KBr instead of Br2.
available solvents: acetone, HAc, eventually chloroform

HLR




View user's profile View All Posts By User
vulture
Forum Gatekeeper
*****




Posts: 3330
Registered: 25-5-2002
Location: France
Member Is Offline

Mood: No Mood

[*] posted on 26-8-2003 at 12:35


2KBr + Cl2 ---> 2KCl + Br2

Cheap, easy, fast, high-yielding only trouble is Cl2 combination.

Just hope it's selective enough towards bromination :P

Or:

2KBr + 2H2SO4 ---> Br2 + SO2 + 2H2O + K2SO4

Separating Br2 and SO2 shouldn't be as difficult.




One shouldn't accept or resort to the mutilation of science to appease the mentally impaired.
View user's profile View All Posts By User

  Go To Top