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Author: Subject: Pictures of your home lab
mewrox99
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[*] posted on 11-6-2010 at 01:15
Pictures of your home lab


Show off your home lab.

Here is mine. It's in my laundry as a temp setup before I get there spare attic room.



P6110001.JPG - 113kB P6110005.JPG - 123kB P6110009.JPG - 143kB P6110010.JPG - 151kB

[Edited on 11-6-2010 by mewrox99]




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JohnWW
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[*] posted on 11-6-2010 at 05:03


Mewrox, thanks for sharing, although you obviously need a lot more equipment, especially distillation apparatus and analytical instruments, and many more reagents, before you can do any really serious chemistry. Oh, and I hope that the corrupt New Zealand Pigs, who oppress us, do not recognize the scenes depicted in your photos, possibly using Google-Earth, and use them as evidence to concoct an excuse to raid you on the pretext of making drugs!

[Edited on 11-6-10 by JohnWW]
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entropy51
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[*] posted on 11-6-2010 at 06:15


JohnWorryWart,

Have you taken your galantamine today?
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DJF90
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[*] posted on 11-6-2010 at 08:09


Quote:
although you obviously need a lot more equipment, especially distillation apparatus and analytical instruments, and many more reagents, before you can do any really serious chemistry.


Don't be so hard on the guy, he's made a good start and thats more than many of us have done!

Quote:
Oh, and I hope that the corrupt New Zealand Pigs, who oppress us, do not recognize the scenes depicted in your photos, possibly using Google-Earth, and use them as evidence to concoct an excuse to raid you on the pretext of making drugs


You're being ridiculous John, like they can see in his laundry room from google earth with any detail(/at all).
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Skyjumper
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[*] posted on 11-6-2010 at 17:58


I'l pop a few pics on monday of the lab I work in. Full fume hood and 4 8foot tall cabinets filled with chems.
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mewrox99
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[*] posted on 11-6-2010 at 20:22


Yeah. My lab is really new. I only made it a week and a half ago. I'm getting some more reagents in the mail. Sodium Acetate, Strontium Nitrate, Barium Nitrate, Potassium Permanganate and I'll be making some sodium metasilicate some time soon.

[Edited on 12-6-2010 by mewrox99]




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JohnWW
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[*] posted on 11-6-2010 at 20:56


Where in New Zealand are you buying those reagents, Mewrox99? Do they ask any awkward questions?
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mewrox99
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[*] posted on 11-6-2010 at 20:59


I so far haven't bought my reagent from real companies.

Trademe, OTC sources, sometimes if it's rare I'll beg my chem teacher who often gives me stuff.

On trademe, countingsheep1 will sell you stuff through email if you have bought alot from him.

Clarks Products LTD sell to individuals but it's bulk technical grade.

HMS-Beagle sell internationally




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psychokinetic
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[*] posted on 11-6-2010 at 22:43


So countingsheep1 is reliable? That's good to hear. He has a lot I like the look of.

*uses his csi skills to see the reflection in the beakers, to see your eyes which can't be made out, but somehow I can see the reflection of your outdoor area. I then take that image and scan it into my computer arbitrarily, push a few buttons seemingly at random and watch as a million images flash on my screen for no reason, as there's no point in downloading all the wrong answers. I then send out a team of analysts who really have no power over you, and one ominously pulls off his sunglasses and makes a bad joke*




“If Edison had a needle to find in a haystack, he would proceed at once with the diligence of the bee to examine straw after straw until he found the object of his search.
I was a sorry witness of such doings, knowing that a little theory and calculation would have saved him ninety per cent of his labor.”
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mewrox99
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[*] posted on 11-6-2010 at 22:48


Quote: Originally posted by psychokinetic  
So countingsheep1 is reliable? That's good to hear. He has a lot I like the look of.

*uses his csi skills to see the reflection in the beakers, to see your eyes which can't be made out, but somehow I can see the reflection of your outdoor area. I then take that image and scan it into my computer arbitrarily, push a few buttons seemingly at random and watch as a million images flash on my screen for no reason, as there's no point in downloading all the wrong answers. I then send out a team of analysts who really have no power over you, and one ominously pulls off his sunglasses and makes a bad joke*


Yeah, Countingsheep1 is reliable I've bought many items from him although at times he can be a wee-bit slow.

Anyway lol wut




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Chainhit222
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[*] posted on 12-6-2010 at 14:14


I have been slowly working on it for a while.
http://www.sciencemadness.org/talk/viewthread.php?tid=12868#...

Current Picture:
http://img155.imageshack.us/img155/1986/labncurrent.jpg

I put all the equipment that would fit into the little filing-shelf by the fume hood. I want to get some nice lockers for the large equipments so its not laying on shelves exposed to the dust. I am a bit lacking in the reagents department too :(.
The acids are stored in the tupaware container under the desk, in case a bottle magically breaks.
But... CL-20, I'm coming for you!



[Edited on 12-6-2010 by Chainhit222]




The practice of storing bottles of milk or beer in laboratory refrigerators is to be strongly condemned encouraged
-Vogels Textbook of Practical Organic Chemistry
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mewrox99
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[*] posted on 16-7-2010 at 03:21


My collection of chems has grown quite bit. And this doesn't include the oxidants and I have ordered some metals (Al, Mg, Zn)



chemicals.jpg - 75kB




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JohnWW
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[*] posted on 16-7-2010 at 10:34


Oh good, with those you will be able to do your own organic reductions using H2 generated by the action of an acid on those metals, and make (using organic halides) your own Grignard reagents for additive organic syntheses.
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mewrox99
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[*] posted on 19-7-2010 at 02:25


Still very inexperienced in O-Chem (I'm only 14)

I'll be making some ethanediamide soon, since that seems simple enough.

Maybe at the start of next year I'll get some distillation equipment, and a magnetic stirrer




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Sedit
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[*] posted on 19-7-2010 at 14:15


IF you don' mind me asking which route do you plan on taking to getto EDA? Iv had my sights on this for a while and was curious as to hw you want t go about it. My idea was to brominate ethylene glycol and pass the Dibromoethane into and excess of (aq)NH3 to yeild EDA*(HBr)2. If you feel its off topic PM me.




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smaerd
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[*] posted on 20-7-2010 at 15:23


<img src="http://i933.photobucket.com/albums/ad173/smaerdsdreams/73e8485a.jpg"/>
<img src="http://i933.photobucket.com/albums/ad173/smaerdsdreams/1ca3a016.jpg"/>

Finally making some progress on this damn thing. Dig the home made test tube rack? lol
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entropy51
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[*] posted on 20-7-2010 at 16:45


Fire extinguisher: Check

Safety Goggles: Check

You get a thumbs up, my man.

How's the ventilation?
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smaerd
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[*] posted on 20-7-2010 at 17:01


Thanks :).

Ventilation is pretty poor. That's my next step before buying a vacuum I believe. I want to do something like a fume-hood or cabinet. I'm just not sure what I'm going to have to do to get that constructed safely. The nearest door/window to the outside is maybe 10 feet away so that's not too far thankfully. I want to do something nice though, like some kind of hockey court glass or something, but that might be wallet draining. Adequate fan's are seemingly expensive as well.

I mostly need to do some research though :P. Some great threads on fume-hoods on here.
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entropy51
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[*] posted on 20-7-2010 at 17:16


Fume hoods have to be fancy to meet official safety requirements. They need not be so fancy to actually take the fumes outside, especially if you don't work with HCN or phosgene. It doesn't take a lot to remove HCl, NH3 or halogens if you stick to a small scale. If you have a blower that provides adequate air flow you're 90% of the way there. Just avoid ether and carbon disulfide in anything but the best hood. Safety is more a mindset than fancy equipment.
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psychokinetic
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[*] posted on 20-7-2010 at 17:32


I've just moved house, and I have a garage :D

Still setting it up. Need to get the fusebox to stop pinging so I can have a stable power source, and perhaps remove the net curtains and put some blinds up.




“If Edison had a needle to find in a haystack, he would proceed at once with the diligence of the bee to examine straw after straw until he found the object of his search.
I was a sorry witness of such doings, knowing that a little theory and calculation would have saved him ninety per cent of his labor.”
-Tesla
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entropy51
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[*] posted on 20-7-2010 at 17:34


Garage good! Blinds even better!
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psychokinetic
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[*] posted on 20-7-2010 at 17:43


Yeah, my 6th form chemistry teacher showed me well what happens to light curtains in a chemistry lab....

If I get off my arse today, I might actually contribute to the topic of this thread, and show pictures of what was already set up in the garage before I moved.




“If Edison had a needle to find in a haystack, he would proceed at once with the diligence of the bee to examine straw after straw until he found the object of his search.
I was a sorry witness of such doings, knowing that a little theory and calculation would have saved him ninety per cent of his labor.”
-Tesla
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Magpie
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[*] posted on 20-7-2010 at 17:47


Quote: Originally posted by smaerd  
Dig the home made test tube rack? lol


Yes, I like the test tube rack. That was the first piece of equipment I made for my lab.

I also like the Morton salt. I have that too, labeled "For lab use only" :D

A lot of my larger utensils came from my wife's kitchen and are now labeled "For lab use only." Dinner plate, sauce bowl, stainless steel bowl, coffee grinder, etc. Today I grabbed her turkey baster! Of course I replace all her stuff with new.
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psychokinetic
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[*] posted on 20-7-2010 at 17:53


Do you label her stuff "For Mrs. Magpie's use only"?



“If Edison had a needle to find in a haystack, he would proceed at once with the diligence of the bee to examine straw after straw until he found the object of his search.
I was a sorry witness of such doings, knowing that a little theory and calculation would have saved him ninety per cent of his labor.”
-Tesla
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Magpie
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[*] posted on 20-7-2010 at 18:56


Quote: Originally posted by psychokinetic  
Do you label her stuff "For Mrs. Magpie's use only"?


That's a default position for utensils located in the kitchen, so labeling is not necessary. She does understand, however that the needs of the lab sometimes take precedence over mere eating.
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