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TheMrbunGee
Hazard to Others
Posts: 364
Registered: 13-7-2016
Location: EU
Member Is Offline
Mood: Phosphorising
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Formaldehyde 36-38%, purified , 3L, CAS# 50-00-0 - €15.83
Calcium Hypochlorite laboratory grade, 1kg, CAS# 7778-54-3 - €10.62
Methanol pure for analysis - min 99.8%, 5L, CAS# 67-56-1 - €25.46
Hexane pure for analysis - min 99%, 1L, CAS# 110-54-3 - €32.32
Oxalic acid dihydrate, min 99,5%, 1kg, CAS# 6153-56-6 - €10.92
Cyclohexane, pure - min 99%, 1L, CAS# 110-82-7 - €14.28
Activated carbon beads (highly porous), 500g, CAS# 7440-44-0 - €10.12
Iron(III) Oxide, pure for analysis – min 97%, 1kg, CAS# 1309-37-1 - €13.66
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B(a)P
International Hazard
Posts: 1139
Registered: 29-9-2019
Member Is Offline
Mood: Festive
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Just received 20 g of silver rod and 1 g and platinum rod. Very happy, thanks very much draculic acid69!
Edit, so excited I got the mass wrong
[Edited on 3-4-2020 by B(a)P]
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Cou
National Hazard
Posts: 958
Registered: 16-5-2013
Member Is Offline
Mood: Mad Scientist
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Just received a bottle of 500 grams of benzophenone, for grignard reactions and drying ether
waiting for sodium metal and potassium hydroxide for drying ether
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j_sum1
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Thread Split
12-4-2020 at 03:25 |
woelen
Super Administrator
Posts: 8012
Registered: 20-8-2005
Location: Netherlands
Member Is Offline
Mood: interested
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I cam across some so-called "new old stock" chemicals. Material, which is old, never used, and still in unopened original package. Some chemicals,
which you normally cannot find easily:
sodium arsenate
methylamine HCl
phenolphtaleine powder
sodium chloroacetate
urea (analytical grade, not the greasy prills you normally can buy as fertilizer)
Best thing is the very low price for these chemicals.
The methylamine HCl can be useful for making methylamine easily. Just mixing with NaOH and gently heating drives off the gas and allows me to do
experiments with that. No problem where I live, methylamine is not forbidden in NL.
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Cou
National Hazard
Posts: 958
Registered: 16-5-2013
Member Is Offline
Mood: Mad Scientist
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Choline chloride and glycerin for extracting alcohols from crude esters. https://www.sciencedirect.com/science/article/pii/S004040391...
Holy Sh*t, I wouldn't touch sodium arsenate with a 60 foot pole!
[Edited on 20-4-2020 by Cou]
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valeg96
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Posts: 254
Registered: 6-4-2014
Location: Italy
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Mood: Moodless
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[Edited on 21-4-2020 by valeg96]
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mackolol
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Posts: 459
Registered: 26-10-2017
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Mood: Funky
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Here in Poland I have one very good seller that I order usually from. He has small company offering small quantities of reagents in low price for
experiments. One can as well order bigger quantities with discount. This company has wide choice of reagents and what's funny about it, that the
reagents are packed in urine containers, some in milk bottles and some in cheap plastic or glass bottles. It looks very oldschool and has its climate
and although it is packed in such way, the reagents are good grade. The seller is also very communicative.
Lately I ordered from him anhydrous AlCl3, which was little above 2 times cheaper than normally in Poland and i'm very pleased with the order.
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Refinery
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Posts: 371
Registered: 17-2-2014
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Mood: Still
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Not necessarily on this topic, but is it forbidden to trade stuff on this forum or request any specific items from other users?
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woelen
Super Administrator
Posts: 8012
Registered: 20-8-2005
Location: Netherlands
Member Is Offline
Mood: interested
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Quote: Originally posted by woelen  | I cam across some so-called "new old stock" chemicals. Material, which is old, never used, and still in unopened original package. Some chemicals,
which you normally cannot find easily:
sodium arsenate
methylamine HCl
phenolphtaleine powder
sodium chloroacetate
urea (analytical grade, not the greasy prills you normally can buy as fertilizer)
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Unfortunately I'll have to wait. The seller's postal service does not ship abroad anymore, due to the Covid-19 crisis. The seller will check out at
regular intervals, but till that time he cannot ship the materials. I ordered some other stuff at the same seller in February and that order still
could be shipped, but now I'll have to wait for an unknown period of time 
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j_sum1
Administrator
Posts: 6320
Registered: 4-10-2014
Location: At home
Member Is Offline
Mood: Most of the ducks are in a row
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Nothing particularly special. But I have been so inactive of late every little thing is noteworthy.
I ordered a kg of Al powder from auschems. I found a couple of other items already stored in my basket from waay back: some ammonium carbonate and
benzoic acid. No immediate plans but good to have some basics. Now, if only they had some zinc powder in stock. I am nearly out.
Of course I wishlisted a bunch of other items that I have no need for but will probably get when I have spare cash.
Arrived within 4 days. Auschems is pretty darned good.
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teodor
National Hazard
Posts: 876
Registered: 28-6-2019
Location: Heerenveen
Member Is Offline
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This is "DPD 1" pills for pools. I believe it is N,N-Diethyl-p-phenylenediamine and I need it for the purpose of quantitative chlorine analysis in gas
experiments.
I am not sure whether is it a pure compound or some mix, but it is easily available, so I will try.
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Lion850
National Hazard
Posts: 517
Registered: 7-10-2019
Location: Australia
Member Is Offline
Mood: Great
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Got some calcium bromide CaBr2.xH2O yesterday. For making metal bromide salts by double displacement with the metal sulphates. I wanted 100g but the
supplier only had 500g bottles available so if anyone in my area wants to buy some off me just message me....
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j_sum1
Administrator
Posts: 6320
Registered: 4-10-2014
Location: At home
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Mood: Most of the ducks are in a row
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| Quote: Originally posted by teodor | This is "DPD 1" pills for pools. I believe it is N,N-Diethyl-p-phenylenediamine and I need it for the purpose of quantitative chlorine analysis in gas
experiments.
I am not sure whether is it a pure compound or some mix, but it is easily available, so I will try. |
I was wondering what was in these but had not got around to looking it up.
The cheapest I have seen them is $0.12 per pill which is good enough for intended use but not a great price for bulk. But if you are using it as an
indicator, you might not need too much.
Do start a thread to let us know how your experiment goes. I am sure I am not the only one interested.
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Lion850
National Hazard
Posts: 517
Registered: 7-10-2019
Location: Australia
Member Is Offline
Mood: Great
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Today I received fine nickel powder (100g) and food grade calcium acetate (200g). Nickel powder to try and make nickel iodide one day, and the calcium
acetate to give me a route to make metal acetates by double displacement of metal sulphates with the calcium acetate.
Also ordered sodium molybdate on eBay, as price seemed to good to pass on. But not arrived yet.
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DavidJR
National Hazard
Posts: 908
Registered: 1-1-2018
Location: Scotland
Member Is Offline
Mood: Tired
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Recent orders:
1kg oxone ("potassium peroxymonosulfate", but more accurately 2KHSO5·KHSO4·K2SO4).
10g dendritic samarium
100g nickel (II) sulfate heptahydrate
100g ammonium ferrocyanide
10g barium hypophosphite
250g metol (p-methylaminophenol sulfate)
500g succinic anhydride, "practical grade"
500g copper sulfate pentahydrate
175ml chloroethane (in a spray can)
250g p-toluidine
100g 2-ethylanthraquinone
100g congo red
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wg48temp9
National Hazard
Posts: 783
Registered: 30-12-2018
Location: not so United Kingdom
Member Is Offline
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My order for a 1/4in stainless steel needle valve arrived today. It cost £5.30 including postage from China. The quality looked reasonable
and it looks like it has a PTFE ring for sealing the stem. On close inspection of the needle its not seating uniformly and when tested in the closed
position it leaks slightly.
https://www.ebay.co.uk/itm/383455916028
I see the price has gone up by about £1
I am wg48 but not on my usual pc hence the temp handle.
Thank goodness for Fleming and the fungi.
Old codger' lives matters, wear a mask and help save them.
Be aware of demagoguery, keep your frontal lobes fully engaged.
I don't know who invented mRNA vaccines but they should get a fancy medal and I hope they made a shed load of money from it.
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karlos³
International Hazard
Posts: 1520
Registered: 10-1-2011
Location: yes!
Member Is Offline
Mood: oxazolidinic 8)
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Not directly an order, as it was a gift from a friend, but I got some nice treats I looked around to acquire instead of isolating them myself.
Actually only wanted the natural allybenzene for my planned synthesis route, but well, now I got some isomerized propenylbenzene of that substance as
well 
I'm talking about apiole and isoapiole, just a few grams each but thats enough for my plans.
With the allylbenzene I plan to brominate it, and then go on to prove the simplest primary amination method to work as expected on that substrate.
A tiny little revolution one could say, since this replaces the use of either benzylamine followed by CTH debenzylation, or the use of NaN3 followed
by reduction to get the primary amine.
No, I will use a cheap, harmless, well working, and very mild method, I will use sodium diformylamide!
I love that gabriel reagent, it is the best really!
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Cou
National Hazard
Posts: 958
Registered: 16-5-2013
Member Is Offline
Mood: Mad Scientist
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| Quote: Originally posted by Refinery | | Not necessarily on this topic, but is it forbidden to trade stuff on this forum or request any specific items from other users?
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No we have some users who sell to SM users, e.g. mario
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monolithic
Hazard to Others
Posts: 436
Registered: 5-3-2018
Member Is Offline
Mood: No Mood
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I just bought 64 oz of Liquid Lightning at WalMart. https://www.walmart.com/ip/Liquid-Lightning-Virgin-Sulfuric-...
Crystal clear color, density was measured as 1.818 g/ml @ 27 C which corresponds to 92-93% w/w. Make sure you buy the white bottle shown in my link,
which is the virgin/unbuffered formula marketed to professionals. The black bottle is impure garbage, dark brown in appearance with buffers and a
concentration (per the MSDS) of something like 44% w/w.
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Draeger
Hazard to Others
Posts: 185
Registered: 31-1-2020
Location: North-Rhine Westfalia, Germany
Member Is Offline
Mood: Slowly getting ready for new projects
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Bought 100g of sulfur granules and 100g of zinc shavings from Onyxmet for 12€ total. Zinc was 5.50€ and sulfur was 2.00€, while shipping was
4.50€.
Collected elements:
Al, Cu, Ga, C (coal), S, Zn, Na
Collected compounds:
Inorganic:
NaOH; NaHCO3; MnCl2; MnCO3; CuSO4; FeSO4; aq. 30-33% HCl; aq. NaClO; aq. 9,5% ammonia; aq. 94-96% H2SO4; aq. 3% H2O2
Organic:
citric acid, sodium acetate, sodium citrate, petroleum, mineral oil
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j_sum1
Administrator
Posts: 6320
Registered: 4-10-2014
Location: At home
Member Is Offline
Mood: Most of the ducks are in a row
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A couple of kg of zinc ordered off ebay which I intend to make into powder.
Nothing remarkable in that but the seller, Toby from gembrookcreek recognised me from this board. I am not used to being recognised. Anyway, we had a
pleasant little interchange via ebay.
FTR, gembookcreek has a few different metals for sale at what seem to be reasonable prices.
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monolithic
Hazard to Others
Posts: 436
Registered: 5-3-2018
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Mood: No Mood
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| Quote: Originally posted by j_sum1 | A couple of kg of zinc ordered off ebay which I intend to make into powder.
Nothing remarkable in that but the seller, Toby from gembrookcreek recognised me from this board. I am not used to being recognised. Anyway, we had a
pleasant little interchange via ebay.
FTR, gembookcreek has a few different metals for sale at what seem to be reasonable prices. |
How do you plan on making the zinc into a powder? Sounds interesting but also sounds like a lot of work.
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j_sum1
Administrator
Posts: 6320
Registered: 4-10-2014
Location: At home
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Mood: Most of the ducks are in a row
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Electrolysis in alkaline solution. Nurdrage has a video on this. He dissolves Zn in NaOH solution and electrolyses with Cu cathide and inert anode.
The fine zinc falls off the copper. I intend to use Zn anode so that the zinc in solution is self replenishing.
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woelen
Super Administrator
Posts: 8012
Registered: 20-8-2005
Location: Netherlands
Member Is Offline
Mood: interested
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| Quote: Originally posted by woelen | | Quote: Originally posted by woelen | I cam across some so-called "new old stock" chemicals. Material, which is old, never used, and still in unopened original package. Some chemicals,
which you normally cannot find easily:
sodium arsenate
methylamine HCl
phenolphtaleine powder
sodium chloroacetate
urea (analytical grade, not the greasy prills you normally can buy as fertilizer)
|
Unfortunately I'll have to wait. The seller's postal service does not ship abroad anymore, due to the Covid-19 crisis. The seller will check out at
regular intervals, but till that time he cannot ship the materials. I ordered some other stuff at the same seller in February and that order still
could be shipped, but now I'll have to wait for an unknown period of time
|
I'm happy with this order again
The material could be shipped, the Covid-19 regulations were loosened. The parcel arrived. I have done my first experiment with the arsenate ion, in
comparison with phosphate ion.
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G-Coupled
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Posts: 287
Registered: 9-3-2017
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Mood: Slightly triturated
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NVM
Sorry.
[Edited on 25-5-2020 by G-Coupled]
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