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Ozone
International Hazard
Posts: 1269
Registered: 28-7-2005
Location: Good Olde USA
Member Is Offline
Mood: Integrated
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I've had good results with these at up to about 160°C. A small stir bar will fit just fine. I will also tell you that if your reaction takes off, it
will strip the threaded plug out of the glass--which remained intact (not so much objects hit by the projectile or the oil bath it was in). You may
also need to clean out your pants.
https://www.ebay.com/itm/Chemglass-15mL-HW-Cylindrical-Press...
O3
-Anyone who never made a mistake never tried anything new.
--Albert Einstein
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semiconductive
Hazard to Others
Posts: 326
Registered: 12-2-2017
Location: Scappoose Oregon, USA.
Member Is Offline
Mood: Explorative
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Those are basically what I want to put the little glass vials inside of to do reacctions. Right now, I can only put them in a steel container that
can withstand explosions with silicone oil over the top to keep the glass vial from taking the pressure by itself .. but with a good pressure
reaction vessel, I'd be able to see the reaction going on inside the disposable glass vial; That way I can see the reaction going on, and if the vial
is still surrounded by silicone oil; even if it's ruined by a burnt chemical or even if it breaks ... the more expensive pressure reaction vessel
should still have a layer of protection.
Thanks, that idea is definitely a step up from what I have.
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