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Author: Subject: Hard to find, high quality reagents and glassware for sale! Rotovaps now available
yobbo II
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[*] posted on 12-1-2025 at 16:43


I think this is an 'Iodine' stopper.

https://www.sciencemadness.org/whisper/files.php?pid=625589&...

How does having a funnel neck allow an airtight seal without grease?

Yob

[Edited on 13-1-2025 by yobbo II]
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drakedevel
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[*] posted on 13-1-2025 at 22:17


Quote: Originally posted by yobbo II  
I think this is an 'Iodine' stopper.

https://www.sciencemadness.org/whisper/files.php?pid=625589&...

How does having a funnel neck allow an airtight seal without grease?

Yob

[Edited on 13-1-2025 by yobbo II]


I agree, that stopper does look like one that goes with an iodine flask.

The wet ground glass joint is what provides the airtight seal, just like with grease. The funnel neck provides a convenient way to get the joint thoroughly wet and supplies a reservoir of excess liquid so evaporation takes longer to compromise the seal.
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SuperOxide
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[*] posted on 15-1-2025 at 03:52


Quote: Originally posted by Texium  
And this is the $5 Bargain Bin. Every piece in these pictures costs $5, and if you order at least $50 worth of chemicals and/or equipment from me, I'll throw one of your choice in for free, while supplies last.



B5A 2000 mL Kimax RBF, neck is broken. Flask has some external scratches/etching.

B5B 500 mL Pyrex Florence flask, no ground glass joint, small crack in the top of the neck but still usable.

B5C 600 mL Pyrex Florence flask, top of neck lip is ground glass as if it was designed to fit flush with another piece and be clamped together

B5D 125 mL Pyrex distilling flask, like-new condition

B5E 250 mL Pyrex iodine flask. Takes 24 mm stopper. Sold

B5F 250 mL Bellco Erlenmeyer flask with extra long, wide neck.

B5G 250 mL heavy-walled Pyrex filter flask with broken hose barb

B5H 200 mL Kimax volumetric flask with unusual flared top

B5I 24/40 Kjeldahl bulb with hose barb outlet

B5J Pyrex gravity chromatography column with fritted disc at bottom and glass stopcock. Will provide fitting stopcock. Sold

B5K Pyrex chromatography column with 125 mL solvent reservoir and glass stopcock. Will provide fitting stopcock. Takes 19 mm stopper, which may be provided if I find more. Sold

B5L 60 mL Pyrex addition funnel with glass stopcock and long stem Sold

B5M ~30 mL addition funnel, angled. Will provide fitting glass stopcock.

B5N Tiny bubbler

B5O 25 mL Dean-Stark trap without ground glass joints. Will provide fitting glass stopcock.

B5P Huge 3-way glass stopcock

B5Q ~1 L Pyrex bottle with 2 24/40 joints

B5R 200 mm Pyrex Vigreux column without ground glass joints.

B5S Large glass tube with 24/40 male joint on one end and 45/50 male joint on other end

B5T Weirdly tall Pyrex 24/40 "h" still head for vertical distillation setup

B5U Pyrex 24/40 odd angled adapter Sold

B5V Unusual Pyrex still head with 2 24/40 male joints and one 19/38 female joint

B5W Kontes 24/40 Y adapter

B5X Pyrex 29/42 tube for cold trap or gas bubbler Sold

B5Y Ace 29/42 tube for cold trap or gas bubbler Sold

B5Z Large Pyrex Dean-Stark trap (?) with male 24/40 joint and female 29/42 joint. Bottom joint is broken but still intact enough to work.

B5AA Strange giant reactor thing. 60/50 center joint, 24/40 and 14/35 side arm joints. Third side arm is broken off.

[Edited on 1-10-2025 by Texium]


Just curious, what could B5S ("Large glass tube with 24/40 male joint on one end and 45/50 male joint on other end") be used for? Im curious why it has two male joints instead of two female joints (but maybe im just more used to seeing tubes with female joints on them)
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Texium
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[*] posted on 15-1-2025 at 11:41


I have no clue, and that is why it is in the bargain bin :D



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Texium
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[*] posted on 19-1-2025 at 14:05
Rotovaps


IMG_3067.jpg - 1.5MB
First off I have 2 Büchi R-200 that are in working condition (one pictured), as well as one R-210 in working condition (pictured) and another one that I'll sell for parts. Vapor duct is included, but I do not have the condensers or water baths for these.

R-200, working, vapor duct included: $300 (2 available)
R-210, working, vapor duct included: $300 (1 available)
R-210, for parts: $150 (1 available)

IMG_3068.jpg - 1.4MB IMG_4272.JPG - 200kB
Next up, I have this Büchi Rotavapor-R (it's so old it doesn't have a model number, but the design is very similar to the R-110). This one has been around the block on this forum. I bought it from Phosphor-ing in 2017 who in turn bought it from Sauron in 2010. It works fine, but I would rather keep a complete R-200 that I have for myself. This one I would like to sell with all the parts included that are shown in that picture on the right:
  • Motor/base
  • Condenser
  • Vapor duct
  • Good condition KD-22 shaft seal
  • 1000 mL collection flask with ball joint and stainless steel clamp
  • Water bath
I'm asking $600 for the lot.

IMG_3062.jpg - 2MB
I also have three more coil condensers of the type that fit the R. The plastic flange ring attached to these is not compatible with the R-200 or R-210, thus I'm selling them separately. $200 each.

IMG_3069.jpg - 1.3MB
Finally, I have a B-461 water bath, which doesn't match any of the rotovap bases I have. I haven't tested it, so I'm not sure it works. If it works, I'll ask $100 for it, if it doesn't, I'd take $50. Let me know if you're interested, and I'll test it.




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They're not really active right now, but here's my YouTube channel and my blog.
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SuperOxide
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[*] posted on 21-1-2025 at 06:21


Btw, I received my order of some 45/50 condensers and reagents from Texium last week - Excellent quality and price. Very happy with my purchase
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