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Author: Subject: Recent bromine synth
lordcookies24
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[*] posted on 24-4-2020 at 19:23


I thought I recognized this thread lol, so weird to see things you forgot you talked about one year ago.
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draculic acid69
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[*] posted on 25-4-2020 at 21:02


Quote: Originally posted by Texium (zts16)  
Quote: Originally posted by outer_limits  
I used KBr/H2SO4/H2O2 method which should also give reasonable yield. But as I mentioned, I've messed up few things which I will improve in next attempt.
Yeah, better cooling should result in a much higher yield. I have gotten up to 84% yield using the same method, but I use a very efficient Graham condenser.


I use a standard 30cm Liebig with ice and water as well as ice/water in a small plastic container for the receiver to sit in.
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