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Author: Subject: Building a DIY Pirani Gauge from a lightbulb
Ubya
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[*] posted on 28-6-2024 at 09:44
Building a DIY Pirani Gauge from a lightbulb



DISCLAIMER

If you copy exactly what I did, you'll be able to read a numeric value that without calibration is nearly useless. I'm ok with nearly useless because i'm only interested in seeing this value going up or down and by how much, the exact numbers are not important to me. If you want to correlate this "random" values to an actual pressure, you'll need to calibrate it with an actual working gauge (that I don't have at the moment).


Objectives of this project


I've been experimenting with plasma discharges for a few years already, and until now I've always totally eyeballed the vacuum level in my systems by just looking at the color and opacity of plasma. A method that worked fine to distinguish if my vacuum chamber or my pump were total garbage, but totally unusable to my untrained eyes to distinguish very minor leaks.
After upgrading to a 2 stages rotary vane vacuum pump, and an all metal KF apparatus, I even got toally rid of any plasma, and was left with fluorescence cause by high energy electrons, but I still needed a way to know if the pressure was going up, down or staying still.

I needed a device capable of distinguishing changes in pressure in the range of 10-1Pa, the lowest pressure achievable by my rotary vane vacuum pump, with junk laying around.
This project doesn't require any particular skills or tools, and all the steps can be done in about 1 hour.

The Pirani Vacuum Gauge

3-A-schematic-diagram-for-Pirani-gauge.png - 19kB


A pirani gauge is essentially a heated filament exposed to the vacuum you want to measure. By feeding a small current to the filament, it will heat up. the amount of heating depends on the supplied current and the pressure of the environment. At higher pressures there are more molecules to carry away the heat from the filament due to convection. At lower pressures there aren't many molecules, and the temperature of the filament increases.
When the filament heats up, its resistance also increases, so we can correlate the increase in resistance with a lowering of pressure.
This resistance change can be very small, not easy to detect with a simple multimeter, so we use a circuit called a Wheatstone Bridge.
wheatstone_bridge_for_calculator.png - 41kB

When R1/R3 is equal to R2/Rx, Vout is 0V.
Any changes in Rx will cause a potential difference to be detected.

My DIY Pirani Vacuum Gauge


Some people wound their own filament from very thin tungsten wire, I thought of doing that too, but I already had a tungsten filament encased in a vacuum tight vessel, just a regular incandescent lightbulb (even though they are pretty uncommon now).

I just had to make a hole in a lightbulb without cracking the glass, easier said than done!
I tried different kinds of lightbulbs, but the best ones are these little miniature lighbulbs that can be had for super cheap.
I bought the 4mm 24V model, and I'll say later why
lightbulb.png - 1MB


After gently sanding the tip with some not so fine sandpaper, I epoxied it in a hole I drilled in a KF25 end cap.
I'm using KF parts because my vacuum system is based on those, but if you are using glass or random copper pipes and jam jars, you can glue this tiny bulb wherever you like, just make sure it is a vacuum tight seal.
Some epoxies don't behave optimally under vacuum. JB-weld is apparently quite good for vacuum work, but I don't have that in my country, so I had to try a few out before I found this that degasses the least.

diy kf pirani gauge top.jpeg - 200kB diy kf pirani gauge bottom.jpeg - 158kB


Now the electrical part of the project.
This are the components I used for the Wheatstone Bridge
- R1 100 ohm 1W
- R3 100 ohm 1W
- R2 220 ohm 1W + 100 ohm potentiometer
- Rx 4mm 24V incandescent lightbulb

diy wheatstone bridge.jpeg - 282kB


R1 and R3 can probably be normal 1/4W resistors, I went with 1W versions only to minimize the resistance change caused by joule heating.

I'm supplying the wheatstone bridge with 5V, so one may ask, why did I buy a 24V rated lightbulb if I'm feeding it with 5V though a resistor of at least 220 ohms.
Tungsten won't melt at 2000°C, but it will happily burn in a blink of an eye if exposed to oxygen.
A bigger temperature delta will give us a bigger resistance delta, and a bigger range of voltages between atmospheric pressure and "vacuum", but it will also shorten the life of our gauge, or instantly kill it as soon as we apply power to it.
The 220 Ohm resistor was picked to make the filament barely glow when under high vacuum, and be only a couple hundred degrees when at atmospheric pressure.
The 100 ohm potentiometer is there for us to set the 0V point at the vacuum lever we desire.

With this configuration the cold filament has a resistance of 60-70 ohm (varies from bulb to bulb) and reaches a max of 320 ohm when heated in a vacuum.
The voltage output goes from -1.2V to 0V.
If in your setup you start getting positive values, it is ok, the pressure is still going down, as i said, these values are arbitrary, their direction is more important than their absolute value.
Still, you can adjust the potentiometer to make your lowest pressure 0V.
If one is bothered by the negative voltage, swapping the leads of the multimeter solves the "issue" XD


Here is a quick video of the gauge in action
Attachment: DIY Pirani Gauge pumping down.mp4 (4.2MB)
This file has been downloaded 12 times

Pirani gauges are intrinsically not very precise, and my rendition of one hasn't for sure the best performance, but it allows me to distinguish changes in pressures of a few Pascals or less

[Edited on 28-6-2024 by Ubya]





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[*] posted on 28-6-2024 at 13:59


Quote: Originally posted by Ubya  

When the filament heats up, its resistance also lowers, so we can correlate the increase in resistance with a lowering of pressure

Raises
But spot on design.
The light bulb filament is the only thing stopping you from calculating the exact pressure.
I would suggest nicrome wire. It is easier to get and more chemically resistant across your desired temperature range. More importantly, you can measure its length accurately. You can not do that with a light bulb filament.(its a spring, made from a spring)
Measuring the length, resistance, and weight you can characterize the heater. Them measure the thermal dissipation and compare it to a reference chart.
stolen from google

Screenshot_20240628_175306_Samsung Internet.jpg - 309kB

As you can see the area useful for radiant thermal emissions is.... more than difficult... to calculate. A stright peace of wire would be much more manageable




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Ubya
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[*] posted on 28-6-2024 at 15:13


Thanks Reinwater for spotting my mistke. Of course I meant increases but I managed to screw up while typing (I had to retype the entire post becase trying to load the video managed to reset the page.....)

Yeah for sure, a more involved design allows a much better control on the various variables, i went with a lightbulb because it is something that anyone can buy and expect similar performances.
I also tried to make metal to glass vacuum tight seals in the past, and it wasn't as easy as I expected.
There are also ways to improve my design, but I went with the simple stupid one, because it is stupid simple to make.

I will try other designs now ;)





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[*] posted on 28-6-2024 at 15:35


This is a nice experiment and I will remember it. I wonder if silicone might work better than epoxy to bond the light bulb to a glass or metal tube. I've been obsessed lately with the potential of silicone cement.
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Ubya
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[*] posted on 28-6-2024 at 15:52


Quote: Originally posted by Jenks  
This is a nice experiment and I will remember it. I wonder if silicone might work better than epoxy to bond the light bulb to a glass or metal tube. I've been obsessed lately with the potential of silicone cement.


I haven't tried any silicone based adhesives in this case, but I've tried using silicone caulking in past vacuum experiments.
It is veeery permeable. I thought I could DIY my own gaskets with silicone, but it was like having a leak





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[*] posted on 28-6-2024 at 18:28


At that pressure, stay away from epoxy, silicone, rubber, steel, zinc, lead, tin, most copper and a long list of other stuff .
Temperature permitting, carving wax also called Faraday Wax will be the cheapest to acquire and easiest to use.
If your wax feels oily, its no good. You want it rock hard at 22c.




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[*] posted on 28-6-2024 at 21:36


Actually nichrome is a terrible choice for a temperature sensing element, as it has a Tcr an order of magnitude less than tungsten (0.0004 vs tungsten's 0.0045). You'd do better with nickel (0.006) or iron (0.005). Or maybe platinum (0.00392) just because it will be more inert, and is available in very thin gauges.

Another way to drive the Pirani gauge is to create a feed back circuit that keeps the gauge wire resistance (and temperature) constant by varying the bridge drive voltage. This keeps the radiated losses constant so only the conduction loss affect the bridge. Bridge voltage is then related to pressure (probably not linear though - these things seldom are). Easy to do with a single opamp.

The only question I have with DIY Pirani gauges is how to calibrate it?

[Edited on 29-6-2024 by Twospoons]




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Ubya
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[*] posted on 29-6-2024 at 01:14


Quote: Originally posted by Twospoons  


The only question I have with DIY Pirani gauges is how to calibrate it?


Exact reason why I added a disclaimer at the top of the post :P





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[*] posted on 29-6-2024 at 02:41


Quote: Originally posted by Ubya  
I just had to make a hole in a lightbulb without cracking the glass, easier said than done!

Glue a small piece of carborundum with epoxy putty to the head of a 2 mm Ø steel nail and attach the nail to a portable screwdriver. The carborundum can come from a sharpening stone or from a thick metal cutting disc.

Edit: By the way, nice idea.

[Edited on 29-6-2024 by bnull]




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[*] posted on 29-6-2024 at 03:43


Quote: Originally posted by bnull  
Quote: Originally posted by Ubya  
I just had to make a hole in a lightbulb without cracking the glass, easier said than done!

Glue a small piece of carborundum with epoxy putty to the head of a 2 mm Ø steel nail and attach the nail to a portable screwdriver. The carborundum can come from a sharpening stone or from a thick metal cutting disc.

Edit: By the way, nice idea.

[Edited on 29-6-2024 by bnull]


I have glass drill bits and diamond coated dremel bits (different shapes).
it mostly depends on the type of bulb how easy is to crack it.
someone also suggested me to try the drilling/sanding under water, but I fear it would damage the delicate filament

probably the best way would be to use the flat side of a diamon coated disc





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[*] posted on 29-6-2024 at 05:41


What about waterproof sandpaper for metal with a little bit of vaseline or mineral oil as lubricant? I never had issues with a 150 grain sandpaper at low speed (<1000 RPM), and the surface gets rough enough to permit a good adhesion.



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[*] posted on 29-6-2024 at 12:06


Quote: Originally posted by bnull  
What about waterproof sandpaper for metal with a little bit of vaseline or mineral oil as lubricant? I never had issues with a 150 grain sandpaper at low speed (<1000 RPM), and the surface gets rough enough to permit a good adhesion.


I ordered more lightbulbs to make other things. I might use the excuse to try different cutting methods.

I didn't want to use oil in this case because it would have been impossible to remove fully without damaging the filament (maybe soaking for multiple times in clean solvent) or spoiling the epoxy seal or vacuum





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[*] posted on 29-6-2024 at 14:03


On the other hand, you can use the sandpaper dry. Just blow it and the bulb now and then to cool and remove glass dust. It takes a little longer to drill but, again, I never had issues.



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