vibbzlab
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Help in reineck salt synthesis.
Hello fellows
I am looking for a synthesis writeup for reineckes salt. I know it's fusing ammonium thiocyanate and ammonium dichromate . I really want a detailed
explanation.if anyone have a link or writeup please provide
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mayko
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here's the prep from Organic Syntheses:
http://www.orgsyn.org/demo.aspx?prep=CV2P0555
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vibbzlab
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This I had seen. I didn't quite understand the part where it says about dissolving in ice and then boiling water. That part I didn't understand
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UC235
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The insoluble material is saved after the ice water wash. This removes more soluble impurities. The solid is then dissolved in prewarmed water,
heated back to 60C, hot filtered and cooled immediately. Hydrolysis is rapid at high temperatures, the prewarmed water is to reduce the time it
spends at elevated temperatures, but 60C is needed to ensure good solubility for crystallization.
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vibbzlab
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Thank you so much for giving the idea
Amateur chemist. Doctor by profession
Have a small cute home chemistry lab.
Please do check out my lab in YouTube link below
This is my YouTube channel |
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