FriendlyFinger
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Registered: 14-3-2005
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Where did my freebase go?
Swim ran a Al/Hg with 44g P2P and got 86% yield freebase after acid/base.
A few days later swim ran another Al/Hg with 50g P2P and got 16g freebase after
toluene extraction. Where's the other 35 or so grams? The only thing that swim did differently is use 10% NaHCO3 for the washes instead of 5%
NaOH. So where did all that oil go? Did it go out with the wash? Why?
Regards,
FF
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12AX7
Post Harlot
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| Quote: | Originally posted by FriendlyFinger
Swim ran a Al/Hg |
Swim is...?
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Chris The Great
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swim = Someone Who Isn't Me
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bio2
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Were the ketone and amine from the same batch?
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I am a fish
undersea enforcer
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This is a chemistry forum. It is not the place for "where did my drug synthesis go wrong?" posts. Your previous drug-related posts have
been tolerated, as the topics have been relevant to chemistry as a whole. This however, is going too far.
* Thread Closed *
[Edited on 17-8-2005 by I am a fish]
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