SAM4CH
Hazard to Others
Posts: 162
Registered: 16-7-2004
Location: TA
Member Is Offline
Mood: PERFECT
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Full Design cell for Sodium Perchlorate
I need help in design my perchlorate cell!! I get very good results which I can make 2600g per 4days at 120A and 6Volts with no buffer or HCl added! I
faced many problems in my 6Liter cell like connection and install the lead dioxide anodes "I past it with fiber and epoxy glue but I faced problem
when I like to reinstall new anode if one of them has crack, my anodes number is four and 12mm, 30,5cm Gouging rods coated with 4-5mm PbO2" I need
mechanical and chemical help because in last week my cell explode after 10minutes of operation and I think that cause of hydrogen gas but I let
Hydrogen to escape through 20mm hole, and my cell provided with Exhaust Fans..
my current cell has these dimensions :
5cm width * 25 hight *50 long cm the case is stainless steel 304 and it is cathode (-)
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FrankRizzo
Hazard to Others
Posts: 204
Registered: 9-2-2004
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Mood: No Mood
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Would you mind posting photos of your setup? Also, what are you using for such a high current power supply?
[Edited on 14-1-2007 by FrankRizzo]
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chloric1
International Hazard
Posts: 1142
Registered: 8-10-2003
Location: GroupVII of the periodic table
Member Is Offline
Mood: Stoichiometrically Balanced
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Shoot I wouldn't mind having a photo of the exploding cell 
Fellow molecular manipulator
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