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Raid
Hazard to Everyone
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thanks arkoma
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arkoma
Redneck Overlord
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Posts: 1763
Registered: 3-2-2014
Location: On a Big Blue Marble hurtling through space
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Mood: украї́нська
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https://www.youtube.com/watch?v=NIVkBs7oWDI
NileRed just posted this today.
The Etard.
"We believe the knowledge and cultural heritage of mankind should be accessible to all people around the world, regardless of their wealth, social
status, nationality, citizenship, etc" z-lib
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paulll
Hazard to Others
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Mood: It's fine. Really.
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I got a bit excited when I saw, "paint thinner to cherry soda;" A new nilered about something that's actually useful. Realised right before he said it
that of *COURSE* he would be busting out his Chromyl Chloride and this wasn't exactly going to be super-practical. Interesting stuff, though.
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Raid
Hazard to Everyone
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I wonder if I should try what NileRed is doing, I have all the reagents and I seems easy.
Edit: I'm also kinda low on ideas for stuff to do, If anyone has any ideas it would be greatly appreciated.
[Edited on 13-6-2023 by Raid]
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Herr Haber
International Hazard
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You can probably skip the "drink my own pee" step ![:)](./images/smilies/smile.gif)
That being said, I liked the last video a lot. It felt more like his older content: less drama /acting, more chemistry.
The spirit of adventure was upon me. Having nitric acid and copper, I had only to learn what the words 'act upon' meant. - Ira Remsen
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foxofax474
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Registered: 17-4-2023
Location: USA
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Mood: Still processing
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Instead of doing etard for benzaldehyde, maybe do the Sommelet reaction lol since it’s much cleaner and uses less carcinogens
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MrDoctor
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Just thought id mention, i have had success using manganous ammonium alum from the electrolysis of manganese ammonium sulfate, more or less prepared
according to the patent on, oxidation of alcoholic chocolates, i think? either way its not difficult at all, its a simple double salt that
precipitates easily and can then be recharged endlessly by electrolysis using lead electrodes.
Its a PITA to handle though. when electrolyzed, it essentially condenses, as these massive molecules, which is probably why its not able to
over-oxidize alcohols unless in a very dilute solution. Anyway, it precipitates and becomes difficult to stir, then you would add your alcohol, in my
case toluene, heat it to a reflux temp and, pretty much just do that until it changes from its beautiful purple to its inactive cream color. upon
reacting much but not all of it, dissolves into solution again.
the messy part is this, you now have an acidic sludge that you need to do a solvent extraction from to get your aldehyde. and due to the massive
molecular weight, you need about a liter of sludge for about 30ml of product. its advised to just steam distill anything out, and make the reactor one
you could steam distill out of, while also performing the electro-regeneration in. otherwise you need a neutral solvent to pull most of the product
out with and just deal with having to do loads of distillation.
i forget where, it might be these forums, but a potassium double salt (no its not potassium permanganate XD) was discovered as well that could do the
oxidation with far less heating, allowing for much lower BP alcohols to be oxidized.
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