argox120
Harmless
Posts: 20
Registered: 3-1-2022
Member Is Offline
|
|
Hydroiodic acid and sodium ethoxide/butoxide sources
would like to get my hands on these reagents"
Hydroiodic acid(250-500ml) and sodium ethoxide or sodium tertbutoxide(100g-250g) for a reduction of teriary alcohol.
|
|
|
Sir_Gawain
Hazard to Others
Posts: 457
Registered: 12-10-2022
Location: [REDACTED]
Member Is Offline
Mood: Stable
|
|
Are you unable to make them yourself? That’s likely going to be easier than buying.
“Alchemy is trying to turn things yellow; chemistry is trying to avoid things turning yellow.” -Tom deP.
|
|
|
j_sum1
Administrator
Posts: 6333
Registered: 4-10-2014
Location: At home
Member Is Offline
Mood: Most of the ducks are in a row
|
|
Duplicate thread. I am closing the other one.
|
|
|
bnull
Hazard to Others
Posts: 475
Registered: 15-1-2024
Location: South of the border, wherever the border is.
Member Is Offline
Mood: Fighting the banking system and international commerce. Still losing.
|
|
There are other routes available that don't make use of HI or EtONa. What tertiary alcohol is it?
Quod scripsi, scripsi.
B. N. Ull
P.S.: Did you know that we have a Library?
|
|
|
argox120
Harmless
Posts: 20
Registered: 3-1-2022
Member Is Offline
|
|
it is a benzylic tertiary alchol like 1,1 dimethyl benzyl alcohol
|
|
|
bnull
Hazard to Others
Posts: 475
Registered: 15-1-2024
Location: South of the border, wherever the border is.
Member Is Offline
Mood: Fighting the banking system and international commerce. Still losing.
|
|
2-phenyl‐2-propanol, eh? Trying to make cumene and analogues?
What about generating HI in situ?
I remember seeing something for tertiary alcohols, like a Wolff-Kischner. Are you following a published procedure?
I ask those questions because there're probably other ways that don't need HI or EtONa.
Quod scripsi, scripsi.
B. N. Ull
P.S.: Did you know that we have a Library?
|
|
|
Random
International Hazard
Posts: 1120
Registered: 7-5-2010
Location: In ur closet
Member Is Offline
Mood: Energetic
|
|
Does it need to be Sodium Ethoxide or can Magnesium Ethoxide be used?
|
|
|
thermochromic
Harmless
Posts: 17
Registered: 17-1-2018
Member Is Offline
Mood: No Mood
|
|
Just make the HI... your not going to find a legit company willing to sell it to you... either in situ or there is a super easy synth over on Rhodium
|
|
|
![[*]](images/xpblue/default_icon.gif){kind=icon}
