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Author: Subject: Adapting non-quickfit to quickfit glassware
hasani10
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[*] posted on 30-10-2022 at 04:26
Adapting non-quickfit to quickfit glassware


I've recently found a cheap source for some large rbfs and conical flasks, but they don't have ground glass joints. I want to get them as it would save me some cash compared to getting the same sizes at 24/29.

Is there an adapter you can use to go from non-ground glassware to ground glassware? I'm imagining just like a simple thing you'd put in a bung with a female adapter to 24/29 but not quite sure what to search to find it online.

Also, would doing this affect how a distillation/ reflux runs much? Compared to using ground glass joints.

Thanks kindly :)
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Sulaiman
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[*] posted on 30-10-2022 at 04:56


Other than ptfe, resin/rubber/plastic compositions have various chemical compatibility issues with common solvents, acids, bases, oxidisers etc. so choose your materials carefully.

For simple distillation (no reflux) you could use a stopper with a hole and something like
https://laboyglass.com/glass-straight-inlet-adapter-with-24-...

For refluxing or fractional distillation the gas/vapour has to go up while liquid is falling down,
a hole as small as in the adapter above would choke.

I would rather have two ground glass RBFs than five plain neck RBFs - if of similar cost.

PS I have literally dozens of used PYREX flasks with plain necks - part of a job lot - one day they may be useful - one day...




CAUTION : Hobby Chemist, not Professional or even Amateur
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[*] posted on 30-10-2022 at 07:59


They’re cheap because they’re virtually useless (the RBFs anyway, the conical flasks are good to have)



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Dr.Bob
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[*] posted on 30-10-2022 at 12:25


Yes, it is hard to make non-jointed glassware work for real distillations or complex reaction (inert, multineck, etc).

But there are many reactions that are simply stiring chemicals in a flask, and those work fine in any vessel, I use vials, test tubes, bottles, and other vessels to do simple reactions sometimes, when I have lots of parallel reactinos, or want to test multiple conditions or reagents at one time. So they may be useful, just not for distillations.
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