Opylation
Hazard to Others
Posts: 131
Registered: 30-8-2019
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POCl3 via P2O5 + NaCl in borosilicate glass?
Has anybody prepared phosphoryl chloride via the following method? I found it within a small-scale reagent preparation book and it did site another
author who used an autoclave however the author of this book states that if devoid of all moisture the reagents and reaction products do not harm
borosilicate glass at the reaction temperatures
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zed
International Hazard
Posts: 2284
Registered: 6-9-2008
Location: Great State of Jefferson, City of Portland
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Mood: Semi-repentant Sith Lord
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Yeah. Way I remember it, he utilizes a large test-tube as his reaction vessel.
That test-tube surviving for very many runs, seems unlikely.
Sacrificial test-tube?
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