Sciencemadness Discussion Board

Crucible Materials

JJay - 18-2-2016 at 12:54

I am looking at purchasing some crucibles for doing calcinations and melting small quantities of metals, as well as other high-temperature processes that involve solid reactants and intermediates.

I see zirconia, alumina, graphite, and porcelain crucibles on eBay. Most hobbyists who I know who melt metal like graphite, but I'm not sure how it would fare with oxidizing reactants. I remember using porcelain ones in chemistry classes.

What are the advantages / tradeoffs of various types of crucibles, and what kinds do you suggest keeping around for general use?

zed - 18-2-2016 at 14:43

Graphite with oxidizing reagents? Expect fire.

Magpie - 18-2-2016 at 15:06

I have melted silver in ceramic crucibles that I bought from a gold assay supplier. I believe they are mullite.

JJay - 18-2-2016 at 15:29

Quote: Originally posted by Magpie  
I have melted silver in ceramic crucibles that I bought from a gold assay supplier. I believe they are mullite.


Mullite looks like it would work well as a crucible material. It would also be excellent for tube furnaces.