Sciencemadness Discussion Board

Taking the vacuum off.

NERV - 16-1-2003 at 12:21

I recently got myself a 1-liter vacuum still on E-bay. I wanted to know the proper way to return the still to atmospheric pressure. I have herd that you need have a small bleeder valve to allow the air to enter into the system slowly, but I also heard that you could just pull the tube running to the aspirator off. I would think the second method would re-pressurize the glass to fast causing an explosion. What methods do you guys suggest?

a_bab - 17-1-2003 at 05:39

If the tube diameter is small, you can simply pull the tube off. Still you are in danger of cracking the glassware.

Why about bending the tube, allowing
only a small quantity of air to enter ?

rikkitikkitavi - 17-1-2003 at 11:22

or install a t-connectr, adding a tube ending in a screwclip which you can completely close the air flow in and slowly open up , slowly letting air in when finishing the vacuum.

If you have a good vacuum source you can even use it as a course regulation of vacuum.

/rickard