Sciencemadness Discussion Board

Air-Free Inert Atmosphere Starter Kit for the Serious Advanced Oganic Synthetic Chemist

Tkuze - 5-6-2019 at 11:44

Here's a list of products with links necessary to obtain the cheapest, most cost effective Air-Free chemical synthesis nitrogen gas setup, adjust to taste. SWIM obtained the exact products ( exception is vacuum tubing diameter-adjust to fit individual regulator outlet/DIY baloon needle luer lock inlet port for filling. Enjoy and feel free to add opinions, your setup, or any questions.
•#20 compressed nitrogen tank with CGA580 female outlet- $128 full after taxes from Airway Oxygen(or order empty on Amazon($85 empty with $30 hazmat fee / from local homebrew store).New 20 cu ft Steel Nitrogen Cylinder with CGA580 Valve https://www.amazon.com/dp/B01E2TC2GO/ref=cm_sw_r_cp_apa_i_9O...
• low flow rate duel Nitrogen regulator(STKUSA Welding Nitrogen Regulator With Pressure Gauge CGA580 Inlet Connection and 1/4-Inch Male Flare Outlet Connection https://www.amazon.com/dp/B07CJ28LCB/ref=cm_sw_r_cp_apa_i_hr...)- $37.
• PTFE vacuum tubing ( only 2" length needed for making baloon apparatus)/ can use HDPE tubing( adjust diametet to individual regulator outlet)- Duda Diesel( ~$10+$11 shipping) http://www.dudadiesel.com/choose_item.php?id=FluoroHose031-F...
• extra thick party baloons( $10 on Amazon).King's deal (Tm) 12 Inches Ultra Thickness Latex Balloon 100 Count - Fuschia, Pink, White, Black, Coffee,orange,assorted Colors (Orange) https://www.amazon.com/dp/B00KBSK9IO/ref=cm_sw_r_cp_apa_i_pE...
• Normject 1mL syringes( green plunger)- $25 on Amazon or Ebay. Plastic Syringe, Luer Slip, 1 mL, PK 100 by Norm-Ject https://www.amazon.com/dp/B01HDYBGNA/ref=cm_sw_r_cp_apa_i_Ww...
• 18-22 guage Stainless Steel veterinary needles(luer lock, fits Norm-Ject)-20PACK 18G 12-30mm Veterinary Stainless Steel Injection Needle,pet Poultry Needle,Bovine Pig Injection Needle https://www.amazon.com/dp/B07G57TKTP/ref=cm_sw_r_cp_apa_i_xz...
• Parafilm- Parafilm M PM996 All Purpose Laboratory Film https://www.amazon.com/dp/B004VQP6CQ/ref=cm_sw_r_cp_apa_i_Fy...
☆ allows one to get about 150-200 full nitrogen baloons ( probably use 2x per average reaction) before refilling
- good luck and always secure your tank to a solid surface to prevent severe bodily harm.

SWIM - 5-6-2019 at 12:37

"SWIM obtained the exact products"

No, I never obtained those products.
Stop making things up about me.

And why is some guy who says he has a professional lab acting like a refugee from the hive? Are you afraid to admit you made a nitrogen atmosphere setup?

Let's see some photos of that real lab space your LLC is located in.
The hoods, the biotage, etc, etc, etc.

You talk mighty big for somebody who's shown us a garage workspace that is lamer than mine and then asked for advice on improving it.



[Edited on 5-6-2019 by SWIM]

[Edited on 5-6-2019 by SWIM]

[Edited on 5-6-2019 by SWIM]

Tkuze - 5-6-2019 at 13:27

Im just giving advice with plausible deniability and separating professional from hobby. The only reason im on here is to spread knowledge. This is stuff i purchased with my own money. All my other stuff was ibtained through grants and external funding, so i cant be advertising those things. I suggest you focus on your own business and not critisize me for no reason. I have dont nothing to you.

Tkuze - 5-6-2019 at 13:38

Heres all the time im wasting on you. If you want to talk science.. then thats fine. But i suggest you dissolve your ego and worry about yourself and bettering the understanding of others using the gift of intelligence and knowledge you have


IMG_0297.JPEG - 1.8MBIMG_0853.JPG - 1.7MBIMG_1263.JPG - 1.5MBIMG_1136.JPG - 2.9MB

Tkuze - 5-6-2019 at 13:55

I can post more pics.. but i dont think you understand the OSHA and EPA regulations and hazardous storage requirements in a professional lab. In a hobby lab, these regulations dont exist.