As for PBr3 you can put phosphorus in bromine, could you do the same in liquefied chlorine ? I mean, generate chlorine, liquefy it on a dry ice bath,
and then put the phosphorus in the chlorine? Would this reaction be very violent?( i have to mention putting a reflux in order to be sure that except
for the first phosphorus drop, there won't be any more significant quantity of oxygen on the reaction flask )Tsjerk - 2-2-2019 at 08:02
Dilute with some inert solvent. fusso - 2-2-2019 at 08:30