Quote: Originally posted by deltaH |
Not so sure what you mean by the ethanol holdup here, can you clarify, please?
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As for the liquid in the thumper, as a poor second stage, it's alcohol content is probably higher than the still and lower than the final distillate
at all times. So towards the end of the run, when the conc. of the alcohol in the still is much lower, then so too would the conc. of the alcohol in
the thumper be, but still higher than the still's. Anyway, the conc. of alcohol recovered in batch distillate starts out high and ends low as well.
It's for the distiller to decide when to stop pulling and so this sets the overall recovery. He decides when to stop because the conc. drops too low
towards the end. The thumper ups conc. by acting as a partial second plate, so that allows the distiller to continue the run a little longer before
reaching the same low conc. of distillate he would have for a single stage... so I would imagine it improves overall recovery in a batch operation,
but that's speculative. Again, it would have been nice to model all this, but none of the free software I have can do non-steady state calculations
for batch distillation.
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This does a better job explaining it than I can. The holdup often leads to mechanical losses due to surface area, especially in packed columns, unless
you feel like washing out all your contact surfaces. |