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Synthesis of longer chain tertiary alcohols
We got 185ml of post-reflux mixture which has a clear upper layer already, without adding any NaOH.
... |
30-12-2015 at 09:28
by: aga |
Synthesis of longer chain tertiary alcohols
[rquote=433377&tid=15171&author=blogfast25]What happened to the rest of the 310 ml of post-r ... |
30-12-2015 at 09:01
by: aga |
Strange Results
Post reflux the liquid was once again a clear colourless liquid.
125ml was spilt off from the rea ... |
30-12-2015 at 07:19
by: aga |
Synthesis of longer chain tertiary alcohols
In 5 minutes the next attempt will have finished refluxing.
This is 20ml alpha-pinene in 40ml 15 ... |
30-12-2015 at 06:00
by: aga |
Synthesis of longer chain tertiary alcohols
Get a distillation going to warm the lab up. |
29-12-2015 at 09:13
by: aga |
Mohr's Titration on Your Soil
The samphire will be grown (if the seeds sprout !) under entirely artifical conditions with no soil ... |
28-12-2015 at 23:57
by: aga |
Books for the beginner books (or how to brush up on old studies one has forgotten)
aaaaaaaaand Welcome to Science Madness mrzwing !
Books are Great.
Youtube is good if you have ... |
28-12-2015 at 13:08
by: aga |
Chemistry Goals, 2016
Pick one and actually Do It.
#7 RFNA is a good one.
It is pretty straightforward, so easily ac ... |
28-12-2015 at 12:40
by: aga |
Mohr's Titration on Your Soil
Today some samphire seeds arrived, and it would be useful to know the NaCl concentration in soil fro ... |
28-12-2015 at 10:41
by: aga |
Synthesis of longer chain tertiary alcohols
It does seem to my barely trained eye that this synthesis has not been thoroughly investigated ... Y ... |
27-12-2015 at 14:34
by: aga |
Synthesis of longer chain tertiary alcohols
OK.
Boiling off the acetone appears to have knackered the product, or at least reduced yield to ... |
27-12-2015 at 11:20
by: aga |
Synthesis of longer chain tertiary alcohols
lol |
27-12-2015 at 09:09
by: aga |
Synthesis of longer chain tertiary alcohols
I only have furry Pets.
Petrol distillation ? OK !
I'll use the Bigger burner. |
27-12-2015 at 09:05
by: aga |
Synthesis of longer chain tertiary alcohols
Some crystals have formed in the 'product' overnight.
[file]46715[/file] |
27-12-2015 at 06:32
by: aga |
Synthesis of longer chain tertiary alcohols
Ok.
We will have to await the Master's pronouncement then.
(Damn. I like making S[sub]2[/sub]C ... |
26-12-2015 at 14:10
by: aga |
Synthesis of longer chain tertiary alcohols
Hold on a sec.
Would directly chlorinating the sodium benzoate not give NaCl and benzoyl chloride ... |
26-12-2015 at 13:51
by: aga |
Synthesis of longer chain tertiary alcohols
[rquote=432911&tid=15171&author=gdflp]Great, conversion to benzoic acid is as easy as dissol ... |
26-12-2015 at 13:39
by: aga |
Clan labs?
There are a limited number of possibilities :-
Scenario A : Chef is actually an anti-drug armed f ... |
26-12-2015 at 13:29
by: aga |
Synthesis of longer chain tertiary alcohols
Got some sodium benzoate if that helps.
Edit:
Might be a good idea to redo the whole thing and ... |
26-12-2015 at 13:06
by: aga |
DemonsHeadshot's thread of many questions
[rquote=432904&tid=64810&author=stygian]at a temperature of iooI to° C.[/rquote]
Erm, are ... |
26-12-2015 at 11:35
by: aga |
DemonsHeadshot's thread of many questions
This an Organic Chemistry question, however there is no procedure, no reference, no homework, no way ... |
26-12-2015 at 11:20
by: aga |
Synthesis of longer chain tertiary alcohols
[rquote=432891&tid=15171&author=blogfast25]For any follow-ups it would be wise to separate t ... |
26-12-2015 at 11:06
by: aga |
Synthesis of longer chain tertiary alcohols
10ml α-pinene
20ml 15 v/v% H[sub]2[/sub]SO[sub]4[/sub]
125ml acetone
were mixed in a 250ml RB ... |
26-12-2015 at 09:08
by: aga |
Ferrite rings/cores - composition & extraction?
Please delete this then re-post in Beginnings. |
25-12-2015 at 13:09
by: aga |
Auto-ignition point of oils/fuels - what is needed to maintain combustion?
'Burning' in this context is basically reacting the oil with oxygen.
Ignore 'flash points'.
A ... |
25-12-2015 at 12:15
by: aga |
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