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Accidentally Powerful Tetrazole
It's makes DDT too quick to be tetrazene or MTX-1, which was my first guess...hmmm... guanylazide it ... |
20-11-2017 at 12:10
by: nitro-genes |
Cheap way of synthesizing TNP? Am I crazy?
[rquote=497507&tid=78227&author=Bert] I once used oil of wintergreen (methyl salicylate), I ... |
19-11-2017 at 13:01
by: nitro-genes |
DDNP & related compounds: The über thread!
Thanks Philou for explaining the probable cause of the reactivity with butanone. I've used acetone f ... |
11-11-2017 at 13:29
by: nitro-genes |
DDNP & related compounds: The über thread!
Was mainly curious if the nitration of isopicramic could be improved somewhat, any ideas if/how this ... |
3-11-2017 at 14:45
by: nitro-genes |
DDNP & related compounds: The über thread!
No, the salts are supposedly extremely sensitive to friction and can explode upon crystallization, s ... |
2-11-2017 at 05:14
by: nitro-genes |
DDNP & related compounds: The über thread!
Previously I attempted the further nitration of isopicramic acid using KNO3/SA and obtained a small ... |
31-10-2017 at 06:37
by: nitro-genes |
Short question / quick answer - Thread
Thanks Philou, its an interesting question what determines the selectivity of the reductions, not on ... |
31-10-2017 at 04:48
by: nitro-genes |
Short question / quick answer - Thread
The selective reduction of a single nitro group for polynitro arenes is usually performed by the sti ... |
30-10-2017 at 16:03
by: nitro-genes |
Might anthropogenic climate change actually benefit humanity, overall?
Maybe one day we'll all say; "Hey, it's good that we put all that CO2 and methane in the air, or we ... |
12-10-2017 at 12:21
by: nitro-genes |
OTC pyrazole synthesis
Many thanks for the upload, also noticed some info about nitration and nitro-redutions in there, mos ... |
4-10-2017 at 16:02
by: nitro-genes |
DDNP & related compounds: The über thread!
Why the reaction of trinitrophenol and cyanide occurs so readily to form isopurpuric acid is beyond ... |
4-10-2017 at 15:31
by: nitro-genes |
OTC pyrazole synthesis
Nope, couldn't find it either  |
3-10-2017 at 16:10
by: nitro-genes |
5-ATZ(5-Aminotetrazole), the nitrotetrazolate ion and friends
A potassium double salt was also something I tried, though only in combination with Cu(II). Tried by ... |
3-10-2017 at 16:00
by: nitro-genes |
OTC pyrazole synthesis
Brilliant if this would work, great find! A one-pot dehydration, condensation and dehydrogenation in ... |
21-9-2017 at 13:31
by: nitro-genes |
OTC pyrazole synthesis
@Clearly_not_atara:
Your right, got some things mixed up probably regarding the formaldehyde.
... |
17-9-2017 at 15:45
by: nitro-genes |
5-ATZ(5-Aminotetrazole), the nitrotetrazolate ion and friends
This might be something to test indeed, whether silver cyanurate is soluble in ammonia, although any ... |
4-9-2017 at 11:27
by: nitro-genes |
OTC pyrazole synthesis
@sigmatropic, if this route would work it would definitely be the most amateur friendly route compar ... |
3-9-2017 at 11:41
by: nitro-genes |
5-ATZ(5-Aminotetrazole), the nitrotetrazolate ion and friends
Sounds like DBX-1 is even more flame sensitive as lead azide and pretty friction sensitive as well, ... |
3-9-2017 at 03:23
by: nitro-genes |
Melamine dinitrate
Even if it would exist: MTN <--> MDN + HNO3. The MDN in strong nitric could also undergo hydro ... |
3-9-2017 at 02:32
by: nitro-genes |
OTC pyrazole synthesis
There seems to be no topic on the OTC synthesis of pyrazole yet, so with this thread I am hoping for ... |
31-8-2017 at 12:19
by: nitro-genes |
5-ATZ(5-Aminotetrazole), the nitrotetrazolate ion and friends
Very nice! How sensitive is DBX-1 to flame or a glowing splint? Do the properties change upon storag ... |
27-8-2017 at 15:45
by: nitro-genes |
When Chemistry Goes Wrong
Also had an incident with an ammonia generator using diammoniumphosphate instead of ammoniumsulfate, ... |
9-8-2017 at 13:40
by: nitro-genes |
5-ATZ(5-Aminotetrazole), the nitrotetrazolate ion and friends
Could only find some info on the diammonium, sodium, potassium and silver salt of 5-nitraminotetrazo ... |
9-8-2017 at 08:54
by: nitro-genes |
5-ATZ(5-Aminotetrazole), the nitrotetrazolate ion and friends
Probably all very dangerous and stupid ideas ...but...
Could you perform VNS using hydroxylamine ... |
7-8-2017 at 16:53
by: nitro-genes |
5-ATZ(5-Aminotetrazole), the nitrotetrazolate ion and friends
Made an inquiry at Gaylord chemical, said I was looking for CuNTZ, but just got an angry reply back. ... |
3-8-2017 at 14:26
by: nitro-genes |
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