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The Fumed Silica Mystery
Oh, then it should work. I thought you were just lighting a lump of the stuff on fire, not with an a ...
20-5-2021 at 14:41
by: Triflic Acid
The Fumed Silica Mystery
Should be, but don't use activated carbon, that will burn away. Maybe some high temperature polymer.
20-5-2021 at 12:08
by: Triflic Acid
The Fumed Silica Mystery
Ok then, maybe you should try adhering the particles to the surface of something else, similar to ho ...
20-5-2021 at 10:42
by: Triflic Acid
Orthosilicate esters from silica gel
Shoot, maybe an alkoxide salt? That isn't volatile at all.
20-5-2021 at 10:18
by: Triflic Acid
Orthosilicate esters from silica gel
But, assuming that I decide to stick to the first paper(Cheng2000) I posted, since I don't have ammo ...
20-5-2021 at 09:43
by: Triflic Acid
Orthosilicate esters from silica gel
Maybe, but I'm don't really like the idea of having to use HF, since then I can't use a glass system ...
20-5-2021 at 09:14
by: Triflic Acid
The Fumed Silica Mystery
Try using alcohol as the fuel, I think the ash is causing the clumping. Alcohol burns cleaner than k ...
20-5-2021 at 08:14
by: Triflic Acid
Orthosilicate esters from silica gel
I was thinking of using kitty litter silica gel, would that work? Also, sorry about the naming mista ...
20-5-2021 at 06:48
by: Triflic Acid
Orthosilicate esters from silica gel
bump...
19-5-2021 at 17:20
by: Triflic Acid
Making silicon tetrachloride
Update, the prep I’m following calls for teos so I’m going to make that directly instead of maki ...
19-5-2021 at 15:03
by: Triflic Acid
Reaction of elemental potassium with sodium hydroxide
Oh shit, didn’t think of NaK. Might want to use an excess of NaOH then
18-5-2021 at 18:02
by: Triflic Acid
Reaction of elemental potassium with sodium hydroxide
The nurdrage way of making sodium is a bit too long for my liking. So I was wondering if the method ...
18-5-2021 at 15:46
by: Triflic Acid
Orthosilicate esters from silica gel
I'm trying to make TEOS(tetraethyl-orthosilicate) for some experiments, but I don't like the normal ...
18-5-2021 at 07:59
by: Triflic Acid
Making Sodium, a new method?
In the end, for the use I need sodium for, I just need an alkali metal. So, I'll probably try to use ...
16-5-2021 at 08:08
by: Triflic Acid
Making Sodium, a new method?
Making sodium seems fun as well, and the next few things that I want to do all require sodium. So, m ...
15-5-2021 at 09:20
by: Triflic Acid
Making Sodium, a new method?
Would it be possible to dissolve sodium chloride in a solvent such as 1,4 dioxane, and then electrol ...
15-5-2021 at 08:42
by: Triflic Acid
Making silicon tetrachloride
bump
12-5-2021 at 20:19
by: Triflic Acid
Aluminum silicide by heating aluminum powder with silicon powder?
I'm trying to make some silicon tetrachloride without heat, so a silicide compound is my next thing ...
12-5-2021 at 20:10
by: Triflic Acid
Help
Ok. Once I add that, do I have to redistill?
11-5-2021 at 19:53
by: Triflic Acid
Help
I just distilled some pyradine, but the problem is that most of it came over as a 50% azeotrope. Any ...
11-5-2021 at 17:43
by: Triflic Acid
wall wart as power supply for electrolysis
The apple chargers I used to use to power arduinos in the past, so I know that they work as DC adapt ...
11-5-2021 at 07:03
by: Triflic Acid
wall wart as power supply for electrolysis
Maybe try shorturl.at/wGPT4, those look really promising for electrolysis.
11-5-2021 at 06:00
by: Triflic Acid
Aldehyde oxidation
If you want to make some strong NaOCl solution, try adding pool shock to sodium carbonate. Most of e ...
10-5-2021 at 19:15
by: Triflic Acid
Methyl iodide (iodomethane) woes (Red P method)
Maybe do a fractional distillation with a really tall column, maybe like 4 or 5 stacked? Or, you cou ...
10-5-2021 at 13:00
by: Triflic Acid
Making silicon tetrachloride
Would SiI4 really dehydrate sulfuric acid :o I have 100g of silicon lumps coming in the mail today. ...
10-5-2021 at 07:21
by: Triflic Acid
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