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Steel retort design for making Na metal for review
[rquote=187731&tid=14491&author=metalresearcher]FIRST TRY ... FAILED :-(

I just did my fi ...
18-9-2010 at 13:33
by: Formatik
Diiodoacetylene
[rquote=187566&tid=4915&author=madscientist] ... Interestingly, it's supposedly possible to ...
18-9-2010 at 13:07
by: Formatik
Synthesis of Diisopropyl-ether
Senderens (Compt. rend. 179, 1018; 181, 700) made it by distilling a mixture of same parts isopropan ...
11-9-2010 at 19:15
by: Formatik
Grouping of compatible chemicals for storage
That list looks very incomprehensive and poorly done, one could add things like not to store ammoniu ...
7-9-2010 at 19:52
by: Formatik
Help !!!! Hg-Thermometer broken !!!!
I've spilled mercury many times and done all sorts of things against it, once I even trapped a mercu ...
7-9-2010 at 12:50
by: Formatik
Cheap HClO4 should I get
My two cents about it below.

Note if you are going to dilute it and reconcentrate: conc. HClO4 do ...
7-9-2010 at 12:36
by: Formatik
Nitrosyl Perchlorate
Using equal volumes, and adding red fuming nitric acid (d= 1.52g/cc) to azeotropic conc. HClO4 under ...
7-9-2010 at 12:15
by: Formatik
KClO3 and H2SO4 reaction
[rquote=186064&tid=14354&author=The WiZard is In]
Noted in passing :—

Gilbert Gordon & ...
29-8-2010 at 10:41
by: Formatik
Exotic Primaries - Complex Salts
[rquote=186290&tid=1778&author=Chainhit222]http://pubs.acs.org/cen/science/88/8834sci1.html
...
29-8-2010 at 10:29
by: Formatik
explosive nitrite esters
The distillation of nitrite and hydrated ethylsulfate, some water, and just a bit K2CO3 which neutra ...
29-8-2010 at 10:23
by: Formatik
KClO3 and H2SO4 reaction
The interaction of sulfuric acid and potassium chlorate was [url=http://www.sciencemadness.org/talk/ ...
22-8-2010 at 16:53
by: Formatik
Exotic Oxidizers
[rquote=185768&tid=14308&author=Taoiseach] Zinc peroxide, unlike the alkali peroxides, can b ...
22-8-2010 at 16:45
by: Formatik
Exotic Oxidizers
[rquote=185164&tid=14308&author=mewrox99]Anyone done any sugar burns, tests with Al, Mg, or ...
21-8-2010 at 14:09
by: Formatik
H2SO4 by the Lead Chamber Process - success
References in Gmelin verify the reaction goes as thought: when SO2 and Cl2 are led into water, this ...
19-8-2010 at 21:37
by: Formatik
H2SO4 by the Lead Chamber Process - success
[rquote=185381&tid=2824&author=un0me2]SO2 is soluble as all fuck in water - the clathrate is ...
16-8-2010 at 19:47
by: Formatik
H2SO4 by the Lead Chamber Process - success
HCl is more volatile, so all you have to do is heat it, and the H2SO4 stays behind. This ought to de ...
16-8-2010 at 10:44
by: Formatik
Experiments with liquid Nitrogen...
I've frozen an iron pipe (maybe around 4cm in diameter) female attachment in liquid nitrogen. After ...
14-8-2010 at 01:31
by: Formatik
Peculiar smell remains in nose
Nitrogen trichloride does something similar, it is very persistant, and stays in the breathing organ ...
14-8-2010 at 01:20
by: Formatik
Perborate and Pyro
The perborates (also percarbonates and persulfates) also give off ozone chemically when warmed with ...
10-8-2010 at 13:57
by: Formatik
The short questions thread (3)
DMSO doesn't convert to dimethyl sulfate in the body, it does convert to the sulfone though ("MSM", ...
9-8-2010 at 20:35
by: Formatik
oxidation of diols
[rquote=183348&tid=12832&author=blogfast25] The powder was isolated. It doesn't dissolve in ...
30-7-2010 at 20:22
by: Formatik
Preparation of anhydrous AlCl3 in DCM - photos
Yes, liquid, not aqueous HCl. Strong H2SO4 and NH4Cl was used to generate the gas. The HCl liquefied ...
30-7-2010 at 19:53
by: Formatik
Preparation of anhydrous AlCl3 in DCM - photos
Has anyone tried reacting liquid HCl with aluminium to get AlCl3? It sounds easy enough, and powder ...
29-7-2010 at 23:00
by: Formatik
2 quick, but rather random, questions
[rquote=182316&tid=13423&author=Formatik] Lithium hypochlorite is used as a swimming pool di ...
29-7-2010 at 22:52
by: Formatik
Setting up microwave for chemistry
I've used a regular household microwave to dry mostly inorganic salts, like acetates, chlorides, oxi ...
22-7-2010 at 16:42
by: Formatik
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