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Acetic anhydride preparation
From Rhodium:
[quote]Acetic anhydride from sodium acetate, using S2Cl2

Translated from russian b ...
30-11-2005 at 01:18
by: Chris The Great
Nitramide reactions
No reference on the HANA, just popped into my head one day. So I have no clue if it will actually p ...
26-11-2005 at 20:00
by: Chris The Great
Nitramide reactions
Some ideas occured to me recently, about using nitramide to prepare interesting and powerful energet ...
25-11-2005 at 23:26
by: Chris The Great
Does anyone know a synth for Novacaine?
The procedure is for di-[i]n[/i]-butylamine but the [i]n[/i]-butyl bromide could easily be replaced ...
23-11-2005 at 20:10
by: Chris The Great
Does anyone know a synth for Novacaine?
That was me :) I say 100 degrees because I saw a website that said that kind of reaction occurs in ...
22-11-2005 at 21:06
by: Chris The Great
Diphoronepentaperoxide (DPPP)
Phorone doesn't work, it was tried by BASF (I think) who got nothing from it.

If you had it, ...
22-11-2005 at 20:57
by: Chris The Great
SAFETY ISSUES (Unique Issues & Answers)
Plan plan plan! Don't wing it! Things go so much better when you take the time to plan it out ...
19-11-2005 at 12:56
by: Chris The Great
Does anyone know a synth for Novacaine?
I don't think ethylene chlorohydrin can be made with HCl solution, I think high yields are only ...
19-11-2005 at 12:45
by: Chris The Great
Would this actually work?
NaCN in the bowl, HCl in the tank?

I also doubt enough Cl2 would be generated fast enough to kill ...
19-11-2005 at 00:48
by: Chris The Great
Nuclear chemistry
I'm researching MLIS for completely unwholesome purposes at the moment :D

(My school agenda ...
15-11-2005 at 17:15
by: Chris The Great
Confusion over power and velocity.
[quote][i]Originally posted by Deceitful_Frank[/i]
The second charge was much more homogenous due t ...
12-11-2005 at 15:03
by: Chris The Great
E&W Forum stagnating?
I found it hilarious to find you logged onto the E&W forum a few minutes after I read this.

I ...
11-11-2005 at 20:51
by: Chris The Great
keeping a notebook
That is correct, it fizzes when bicarb is poured onto it (my lab bench does this as well but to a mu ...
11-11-2005 at 17:25
by: Chris The Great
Amateur chemistry and school
Everyone who knows me knows that I can and do make explosives as a hobby. I even gave a couple of m ...
11-11-2005 at 17:15
by: Chris The Great
keeping a notebook
I have a bad habit of doing the experiment, and then writing it down afterward, I think sometimes I ...
10-11-2005 at 19:53
by: Chris The Great
Ethylenedinitramine
Ahh, good point! I guess NaF would work then.

What I mean by electrolysis is that the fluorine r ...
6-11-2005 at 20:32
by: Chris The Great
Ethylenedinitramine
Maybe electrolysis with an excess of hydrofluroic acid (sodium hydroxide created from NaF electrolys ...
6-11-2005 at 13:55
by: Chris The Great
Methanesulfonyl chloride
Thanks guys! You've saved me!
Also, thanks to Bromic Acid who found the reference Axt posted ...
6-11-2005 at 13:45
by: Chris The Great
Confusion over power and velocity.
See, I always thought that CO2, with an enthralpy of formation of -94kcal/mol, would give more energ ...
5-11-2005 at 18:59
by: Chris The Great
Methanesulfonyl chloride
R-SO2-Cl

I am searching for a synthesis of methanesulfonyl chloride, or other alkylsulfonyl chlor ...
5-11-2005 at 13:55
by: Chris The Great
Not able to log in with https..........
I'm alive, but getting the same error as everyone else. Haven't noticed the post thing bu ...
2-11-2005 at 16:10
by: Chris The Great
Unconventional Shaped Charges
Very interesting idea with metal powder/resin! I am inclined to try it, as I tried making a cone be ...
28-10-2005 at 14:16
by: Chris The Great
Neglected RDX Process
The nitrating mixture in the patent is 80% nitric acid and 20% sulfur trioxide. I've seen the ...
26-10-2005 at 16:19
by: Chris The Great
Lead Dioxide Electrodes
Couldn't you just use an electrode from a car battery, and regenerate the PbO2 surface of defec ...
25-10-2005 at 14:49
by: Chris The Great
alternative oxidizers for hydrazine production
I think it's because there is always a large amount of ammonia, so that forming NCl3 isn't ...
24-10-2005 at 14:56
by: Chris The Great
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