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NiO > NiCH3COO
AlCl3 might work. Reaction conditions? Don't rightly know.
But, the reaction 3NiO + 2AlCl3---- ... |
11-5-2009 at 00:05
by: zed |
Cleaning Inside of Flask
Well, the soda jerks down at the local greasy spoon used to clean out their oily glass coffee pots, ... |
2-5-2009 at 22:59
by: zed |
Parr Shaker Hydrogenator
I'll try to find out more about pressure and temperature capability. Naturally, I wouldn't suggest ... |
1-5-2009 at 23:49
by: zed |
Parr Shaker Hydrogenator
An interesting premise. Since I've had filter flasks quite hot, at 200C to 300C, under fairly high ... |
1-5-2009 at 15:37
by: zed |
Parr Shaker Hydrogenator
Ah, back to Parr Shakers! I don't disparage them. They have their place. But, under some conditio ... |
1-5-2009 at 00:18
by: zed |
Preparation of Sodium Aluminum Hydride and Lithium Aluminum Hydride
My beloved little grand daughter Munchkinkiss, has suggested to me that one might intimately wrap to ... |
5-4-2009 at 01:45
by: zed |
Need Help from the Pyrotechnics Side
You might Inquire to the folks at Firefox. They have a pretty impressive inventory. They don't list ... |
1-4-2009 at 22:16
by: zed |
Parr Shaker Hydrogenator
Actually, somewhere in Ashby's patents, it suggests that the catalyst can be formed in-situ. I like ... |
31-3-2009 at 21:41
by: zed |
Parr Shaker Hydrogenator
Indeed that was the procedure I found.
From "Advanced Inorganic Chemistry" pg 339, 4th Edition, ... |
31-3-2009 at 16:25
by: zed |
Parr Shaker Hydrogenator
I'll see if I can dig up a reference. I'm pretty sure I know what book it is in, it's just a questi ... |
31-3-2009 at 03:25
by: zed |
Parr Shaker Hydrogenator
Actually, I was referring to LiAlH4 synthesis via Heat/Pressure/Li+Al+2H2+THF.
I've always though ... |
31-3-2009 at 01:38
by: zed |
Parr Shaker Hydrogenator
All true. The Pressure Reactor is far superior. And, it isn't limited to low pressure, low tempera ... |
29-3-2009 at 07:26
by: zed |
Parr Shaker Hydrogenator
Yup! It has indeed, you are correct, yet somehow I missed it on Rhodium. I accessed the document v ... |
28-3-2009 at 18:45
by: zed |
For Sale: LiAlH4 98+% pellets - no dust, easy to handle & store
Yup! It's on the special surveillance list. I am corrected. |
28-3-2009 at 18:20
by: zed |
Parr Shaker Hydrogenator
Ummm. There was a Parr unit at auction on e-bay a few months ago, and it was located near me. I ... |
28-3-2009 at 03:35
by: zed |
For Sale: LiAlH4 98+% pellets - no dust, easy to handle & store
Technically, LAH might be a watched chemical. Were you to peruse the list 1 and list 2 chemicals, y ... |
28-3-2009 at 03:19
by: zed |
2-Bromo-PA into PA
As I recall, producing iso-lysergic acid isn't a terminal problem. The isomerization is reversible. ... |
7-1-2009 at 12:34
by: zed |
2-Bromo-PA into PA
My 14 year-old grand daughter tells me that when she and her friends need Lysergic Acid, and her Swi ... |
25-12-2008 at 12:41
by: zed |
2-Bromo-PA into PA
Geez, is it cheap? If it is, you could try refluxing it with a little Potassium Hydride. That mig ... |
23-12-2008 at 23:45
by: zed |
Methylation of 5-Hydroxytryptophan (5-HTP)
I believe 5-Hydroxytryptophane should be easily methylated, without N-protection.
But, you might ... |
23-12-2008 at 22:39
by: zed |
New High School Teacher looking to outfit a classroom
No point in spending big bucks on burets for a high school chem class. Cheaper is better.
Ideas ar ... |
17-12-2008 at 01:48
by: zed |
New High School Teacher looking to outfit a classroom
Burets appear to be overpriced. Want to do some titrations? Use disposable syringes.
They are g ... |
15-12-2008 at 15:36
by: zed |
How to use AlHg Amalgam on Indole?
B-Nitrostyrenes, the benzene analogs to your Indole intermediate, do not reduce well under basic or ... |
13-12-2008 at 23:57
by: zed |
Another home lab gets busted...
I always assume the worst.
Therefore, I assume your encryption will not hold up.
If U.S. Feder ... |
2-12-2008 at 14:16
by: zed |
got into trouble for experimenting in dorm
You got yourself in a little jam. Since you have no power over school administrators, you aren't in ... |
1-12-2008 at 05:29
by: zed |
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