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CHCl3 and CCl4 Prep Overview
Ah. Mendacity then, it is.
Jokes belong in Whimsy.
However, as promised,
"Thiophosgene in O ... |
4-4-2008 at 22:42
by: Sauron |
CHCl3 and CCl4 Prep Overview
What CWC type agents?
Thiophosgene is not on CWC and I said so. It is a commercially available re ... |
4-4-2008 at 21:44
by: Sauron |
CHCl3 and CCl4 Prep Overview
Your absurd distortion of my statements and demeanor simply underscores your inability to be imparti ... |
4-4-2008 at 21:30
by: Sauron |
CHCl3 and CCl4 Prep Overview
I have deleted as many of my posts as possible in this thread because a forum moderated in so biased ... |
4-4-2008 at 20:52
by: Sauron |
Phthalic Anhydride
As Bill Rotsler used to say:
[b]"Just because you are [i]pArAnOiD[/i], does not mean they aren't ... |
3-4-2008 at 22:42
by: Sauron |
CHCl3 and CCl4 Prep Overview
Ketene, being a carcinogen, is a lot scarier.
If you exhaustively chlorinate MeSCN, you isolate n ... |
3-4-2008 at 21:14
by: Sauron |
Phthalic Anhydride
Phthalic acid itself is not often encountered, phthalic anhydride is ubiquitous. A major intermediat ... |
3-4-2008 at 21:01
by: Sauron |
CHCl3 and CCl4 Prep Overview
Where I am, I cannot buy CHCl3. And I cannot buy CCl4. But I need both. Who says CCl4 is unreactive ... |
3-4-2008 at 19:47
by: Sauron |
Phthalic Anhydride
But, pantone, the spellchecker apparently does not know how to spell phthalic, either.
It is tryi ... |
3-4-2008 at 19:13
by: Sauron |
Phthalic Anhydride
O-xylene can be purchased pure. Mixed xylenes are cheaper but you pay one way, or you pay another wa ... |
3-4-2008 at 14:23
by: Sauron |
CHCl3 and CCl4 Prep Overview
The easiest way I know to prepare methyl chloride (gas) is to react TCT and methanol, liquifying the ... |
3-4-2008 at 13:52
by: Sauron |
CHCl3 and CCl4 Prep Overview
Here's the paper by James in J.Chem.Soc., on which my remarks are based.
One of the ways the reac ... |
3-4-2008 at 09:59
by: Sauron |
CHCl3 and CCl4 Prep Overview
Given an ample supply of materials for a reliable smooth chlorine generator, next we turn to what to ... |
3-4-2008 at 09:16
by: Sauron |
Kugelrohr
Meaningless and futile? Nolo contendere.
But as long as we're here we might as well make big ones ... |
3-4-2008 at 06:57
by: Sauron |
Kugelrohr
Dedication or obsession?
Who dies with the biggest chemistry set, wins. |
3-4-2008 at 03:27
by: Sauron |
TCCA 50 Kg, What to Do with It? Haven't got a Pool!
The drum just arrived a few hours ago. I haven't opened it yet.
I have to get a suitable powder f ... |
2-4-2008 at 23:09
by: Sauron |
Synthesis of phthalocyanine
Be cautioned that phthalimide is a heavy duty teratogen.
Unless you are like me and unlikely to s ... |
2-4-2008 at 22:30
by: Sauron |
TCCA 50 Kg, What to Do with It? Haven't got a Pool!
Thanks for the links.
The first one is only mildly interesting, as I am not sure why acylation wi ... |
2-4-2008 at 20:28
by: Sauron |
TCCA 50 Kg, What to Do with It? Haven't got a Pool!
My TCCA is powdered not granular. I was given the choice, and chose powder. Did I upgefuck?
OK 50 ... |
2-4-2008 at 13:02
by: Sauron |
Kugelrohr
I now have the capability to take stills and HD video. Fume hood installation will be finished mid s ... |
2-4-2008 at 12:16
by: Sauron |
TCCA 50 Kg, What to Do with It? Haven't got a Pool!
How dry is dry?
As garage chemist pointed out if you are going to condense and bottle Cl2 in stee ... |
2-4-2008 at 11:57
by: Sauron |
Kugelrohr
I wonder why I can't edit that post?
Anyway I am now told, this is an air motor and reciprocates ... |
2-4-2008 at 11:29
by: Sauron |
TCCA 50 Kg, What to Do with It? Haven't got a Pool!
I wish it were that easy. No, P2O5 does not react with Cl2 at least not at ordinary temperature.
[E ... |
2-4-2008 at 09:52
by: Sauron |
TCCA 50 Kg, What to Do with It? Haven't got a Pool!
Thanks, woelen. Nice tips. So your advice is to just add the stoichiometric amount of conc HCl to TC ... |
2-4-2008 at 02:45
by: Sauron |
TCCA 50 Kg, What to Do with It? Haven't got a Pool!
There seems to be some diversity of opinion about TCCA vs NaDCCA. I am relying on len1 and garage ch ... |
1-4-2008 at 22:58
by: Sauron |
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