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Is this right?
I have done this synthesis with good results. I don't have access to my notebook right now but IIRC ...
14-9-2013 at 12:33
by: Magpie
Preparation of Benzaldehyde from Benzyl Alcohol
Thanks, DJF90. I wrote this procedure up in 2009 but did not post it until now. The picture I show ...
9-9-2013 at 07:39
by: Magpie
Preparation of Benzaldehyde from Benzyl Alcohol
Thanks Waffles, and thanks for posting the article for use of HNO3. No, I have never tried HNO3 for ...
8-9-2013 at 09:32
by: Magpie
Preparation of Benzaldehyde from Benzyl Alcohol
by Magpie
Sept 7, 2013


[b]Introduction[/b]
This procedure is for the preparation of ~ 19mL of ...
7-9-2013 at 12:55
by: Magpie
Preparation of propionaldehyde
[i]Unitized Experiments in Organic Chemistry[/i], 4th ed by Brewster et al has a preparation for pro ...
6-9-2013 at 15:16
by: Magpie
DHS guide to Unconventional Biological Laboratories
I agree that this article is a gross misrepresentation designed to generate hysteria among the chemi ...
4-9-2013 at 18:56
by: Magpie
My homelab, from the beginning till now.
[rquote=297694&tid=25984&author=DutchChemistryBox]
... The municipality wanted to have a co ...
3-9-2013 at 10:11
by: Magpie
Arsenic from Skutterudite
This may help:

http://www.sciencemadness.org/talk/viewthread.php?tid=12045#pid152058
2-9-2013 at 21:47
by: Magpie
Geology/Geochemistry forum [POLL]
I really don't see what all this fuss about subfora is about anyway. Disciplining new people becaus ...
2-9-2013 at 06:29
by: Magpie
Geology/Geochemistry forum [POLL]
[rquote=297499&tid=25938&author=bfesser] Isn't mathematics sort of something outside of Sci ...
1-9-2013 at 13:24
by: Magpie
Geology/Geochemistry forum [POLL]
I have a friend (ex colleague chemical engineer) who makes jewelry from the semi-precious stones he ...
31-8-2013 at 11:01
by: Magpie
Geology/Geochemistry forum [POLL]
I like geology and minerals. I had a friend with a gold mine and assayed a rock he gave me via fire ...
31-8-2013 at 08:46
by: Magpie
Boiling Stones?
I also use little pieces of a broken clay pot.

I'm interested in the silicon carbide boiling ston ...
30-8-2013 at 12:38
by: Magpie
P2O5 and P4O10
Thanks Pyro for that source. The price looks reasonable.

From what I can tell P4O10 is not liste ...
29-8-2013 at 20:41
by: Magpie
P2O5 and P4O10
[rquote=54115&tid=1779&author=ADP]What type of regulations are currently placed on P2O5 in t ...
29-8-2013 at 10:42
by: Magpie
Found an easy way to make chlorine gas from muriatic acid and bleach
When stating that a gas expands when it cools some mention of the Joule-Thompson effect is in order ...
28-8-2013 at 07:42
by: Magpie
hth spa (shock) and Chloroform
http://www.sciencemadness.org/talk/viewthread.php?tid=19824#pid246294


http://www.sciencemadness ...
26-8-2013 at 21:18
by: Magpie
Called by the police for glassware
[rquote=296211&tid=25711&author=MrHomeScientist]

Glad you got to keep your glassware at l ...
19-8-2013 at 08:57
by: Magpie
Purification of phosphorus -- treatment of WP burns
Nice work Pyro. The last picture looks like two sleeping baby Draculas ;)
15-8-2013 at 12:30
by: Magpie
Preparation of Ammonium Molybdate from Molybdenum Disulfide
Yes, thanks for the correction.
14-8-2013 at 06:55
by: Magpie
Preparation of Ammonium Molybdate from Molybdenum Disulfide
August 13, 2013
by Magpie


[b]A. Introduction[/b]
The applicable reactions appear to be:

2 ...
13-8-2013 at 21:34
by: Magpie
Identyfying copper nitrate hydrates for calculations
For Hexavalent: iodometry. I standardized my reagents using bits of copper wire.

[Edited on 13- ...
13-8-2013 at 11:40
by: Magpie
Identyfying copper nitrate hydrates for calculations
I made some copper nitrate once. I tried to dry it but couldn't due to its strong deliquesence. So ...
13-8-2013 at 10:15
by: Magpie
Conversion of Phthalic Acid to Phthalic Anhydride
August 10, 2013
by Magpie


[b]A. Introduction[/b]
“Phthalic acid can be converted to phthal ...
10-8-2013 at 17:40
by: Magpie
1-butanol dehydrogenation via heated copper
Here's some interesting reading on attempts to make acetaldehyde:

http://www.sciencemadness.org/t ...
30-7-2013 at 13:59
by: Magpie
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