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Problems with a resistive ballast arc furnace (resolved)
This may prove useful:

http://books.google.com/books?id=V4VPAAAAMAAJ&printsec=frontcover& ...
27-10-2013 at 09:36
by: Magpie
Synthesis of Ethyl ß-Naphtholate (Nerolin)
[rquote=304798&tid=23333&author=vulture]
Question: Why the specific warning for methanol? I ...
26-10-2013 at 16:49
by: Magpie
Phenol from Domestically Available Chemicals
Why all the fuss about phenol toxicity - you are not planning on sticking your snoot in it are you?
...
14-10-2013 at 08:14
by: Magpie
chem haters
Here's an anecdote about Michael Faraday relating to the question of "what good is experimentalism?" ...
10-10-2013 at 18:48
by: Magpie
Using CO2 gas for grignard reaction instead of dry ice?
I would love to see that woman doing a Grignard with a Cuisinart demo. ;)

Here's a 24 oz CO2 cyli ...
10-10-2013 at 08:36
by: Magpie
Our Beloved Nitric Acid
The sulfuric acid is basically non-volatile at the temperatures used to distill over the nitric acid ...
8-10-2013 at 19:03
by: Magpie
Using CO2 gas for grignard reaction instead of dry ice?
Another possible source of gaseous CO2 is paintball suppliers - that's where I bought my nice little ...
8-10-2013 at 14:26
by: Magpie
Using CO2 gas for grignard reaction instead of dry ice?
Yes, DJF90, of course the rate of gas sparging can be controlled to fit the situation, ie, scale, he ...
8-10-2013 at 11:18
by: Magpie
Grignard reagent problem
[rquote=302475&tid=18110&author=arsphenamine]Formaldehyde boils at -19C and is very soluble ...
8-10-2013 at 06:07
by: Magpie
Grignard reagent problem
I have no idea if or how much methanol is used in the Thetford product. It was a free flowing powde ...
7-10-2013 at 15:43
by: Magpie
Grignard reagent problem
Here's the results of my attempt to react a Grignard reagent, isopropylMgBr, with formaldehyde from ...
7-10-2013 at 14:51
by: Magpie
Using CO2 gas for grignard reaction instead of dry ice?
In addition to convenience (for most of us) another benefit of dry ice would be its cooling effect. ...
7-10-2013 at 13:51
by: Magpie
Now that is what I call a home lab.
You have (had) a beautiful lab which you surely love. I was horrified to see it trashed and hope tha ...
5-10-2013 at 17:37
by: Magpie
Phenol from Domestically Available Chemicals
[rquote=301986&tid=23930&author=MichiganMadScientist]
My question is: is this phenol? Or di ...
3-10-2013 at 18:54
by: Magpie
Grignard reagent problem
Today I made a Grignard reagent, isopropylMgBr. Since I had no problems I thought I should report m ...
3-10-2013 at 16:16
by: Magpie
Handling of diethyl ether
I have an efficient fume hood and with some awareness can avoid offending the mailman or others out ...
3-10-2013 at 07:52
by: Magpie
Catalytic Converter PGM Recovery
I have not done any research on this myself but what you are saying Violet Sin makes sense, ie, that ...
27-9-2013 at 18:49
by: Magpie
Catalytic Converter PGM Recovery
At some point I would like to experiment with catalytic hydrogenations. I know that some of this ca ...
27-9-2013 at 10:50
by: Magpie
Stirrer Shaft to fit 24/40 and is Acid Resistant
I have a ptfe folding prop type stirrer and bearing for size 19/22. I have used it several times bu ...
27-9-2013 at 10:39
by: Magpie
acetonitrile
Yesterday I prepared a small amount of acetonitrile using the method in Vogel's 3rd (forum library). ...
26-9-2013 at 08:18
by: Magpie
Stirrer Shaft to fit 24/40 and is Acid Resistant
This one specifically says it will fit a 24/40 neck:

http://www.ebay.com/itm/PTFE-stirrer-90mm-b ...
25-9-2013 at 21:03
by: Magpie
Stirrer Shaft to fit 24/40 and is Acid Resistant


see: http://www.ebay.com/itm/Electric-overhead-stirrer-mixer-shaft-7-mm-13-PTFE-/260886473693? ...
25-9-2013 at 18:16
by: Magpie
Seriously, Where To Buy Nitric Acid?
http://www.sciencemadness.org/talk/viewthread.php?tid=13090

I've read that Duda Diesel sells it:
...
17-9-2013 at 18:03
by: Magpie
Is this right?
[rquote=299746&tid=26168&author=Magpie]I have done this synthesis with good results. I don' ...
16-9-2013 at 11:09
by: Magpie
Is this right?
Acetonitrile is made by dehydrating with P4O10.
14-9-2013 at 17:04
by: Magpie
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