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Lab Prep of Diethyl Sulfate
I know that this thread is about [b]making[/b] ethyl sulfate. I became intrigued by this compound w ... |
9-12-2013 at 16:35
by: Magpie |
OrgSyn.org
My problem has been solved and I feel foolish telling the reason. I had the screen expanded too muc ... |
4-12-2013 at 20:17
by: Magpie |
OrgSyn.org
[rquote=309968&tid=27728&author=Marvin]I had problems following old links on chrome on my ne ... |
4-12-2013 at 14:10
by: Magpie |
OrgSyn.org
Is anyone else having trouble using this site? All I can get is the hazard warning statement. |
3-12-2013 at 18:33
by: Magpie |
How to make Carbon Tetrachloride
Thank you zenosx. Indeed this project took time and money, luxuries I now have in my retirement. I ... |
1-12-2013 at 21:07
by: Magpie |
Workbench surface
I do my experiments in my fume hood which has a 304 SS pan for a work surface. It has served me wel ... |
27-11-2013 at 10:17
by: Magpie |
How to make Carbon Tetrachloride
Yesterday I fractionated the product from my latest run at making CCl4 from CHCl3. This run (#3) ut ... |
26-11-2013 at 11:38
by: Magpie |
Tour My Lab
Yes, that looks like a bisected grate in that peak. It would be better if the grate were located a ... |
20-11-2013 at 13:56
by: Magpie |
Tour My Lab
[rquote=306209&tid=4777&author=MrHomeScientist]
I'm trying to figure out my own fume hood s ... |
19-11-2013 at 18:39
by: Magpie |
Buying hydrogen peroxide >3% ??
I can't remember. I'll try to remember to check tomorrow.
-------------------------------------
... |
19-11-2013 at 16:59
by: Magpie |
Buying hydrogen peroxide >3% ??
I can get 35% at my local health food store. It's expensive, however. |
19-11-2013 at 16:17
by: Magpie |
Education in the US - ChemE, OrgChem
The difference between a curriculum in Chem E and one in organic chem is a very big one. From an ac ... |
19-11-2013 at 13:33
by: Magpie |
How to make Carbon Tetrachloride
Here's a couple pictures on my progress toward making CCl4 more effectively.
The 600mm Hempel col ... |
14-11-2013 at 15:26
by: Magpie |
Starting home lab--need to worry??
me: placed 1 lb container of Rooto lye (sodium hydroxide) on counter at check-out of hardware store ... |
12-11-2013 at 21:35
by: Magpie |
Starting home lab--need to worry??
[rquote=307021&tid=27232&author=NiK]So I've been doing a lot of reading on this forum and ot ... |
12-11-2013 at 09:46
by: Magpie |
Vacuum Pump Question
If your tap water is reasonably cold you should be able to pull a vacuum down around 1 psi. Or:
... |
10-11-2013 at 21:36
by: Magpie |
How to emulate lab taps with home equipment?
I kindly suggest that you do a little searching on this forum. This question comes up like clockwor ... |
10-11-2013 at 13:10
by: Magpie |
Science is a pisser
The little droplets that result from high impact of liquids are more common than I had imagined. I ... |
9-11-2013 at 08:34
by: Magpie |
Forum Safety Section?
I too think that the safety warnings ought to be in the preps themselves. Looking back at my Brewst ... |
7-11-2013 at 15:25
by: Magpie |
How to make Carbon Tetrachloride
[rquote=306374&tid=14927&author=deltaH]Hi [b]Magpie[/b], wonderful and courageous effort! I ... |
7-11-2013 at 13:28
by: Magpie |
How to make Carbon Tetrachloride
Len1, in his book "Small-Scale Synthesis of Laboratory Reagents," shows how he converted chloroform ... |
6-11-2013 at 17:01
by: Magpie |
Preparation of cyanides
see:
http://www.sciencemadness.org/talk/viewthread.php?tid=9128&page=2#pid194639 |
6-11-2013 at 14:55
by: Magpie |
Safety equipment
Excellent analogy, quantum. I have been working with a high pressure Hg arc tube recently that prod ... |
2-11-2013 at 13:21
by: Magpie |
Quinone chemistry and absorption spectrum
FYI, some homemade quinones obviously absorbing in the visible spectrum:
http://www.sciencemadnes ... |
31-10-2013 at 12:06
by: Magpie |
On the thermodynamics of phenolic metathesis type reactions... some numbers
I commend deltaH and others (like blogfast) who predict and explain chemistry through thermodynamics ... |
27-10-2013 at 10:14
by: Magpie |
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