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Preparation of Benzyl Chloride
Generally, it is nothing new, see for example this:
http://www.lambdasyn.org/synfiles/benzylchlorid ... |
4-12-2016 at 09:01
by: kmno4 |
Need help recovering alpha-phenylacetoacetonitrile
Another, another run:
Mixure of IPA (5 g) and toluene (~21 cm3) was prepared and 1,3 g of sodium ... |
25-11-2016 at 11:18
by: kmno4 |
Need help recovering alpha-phenylacetoacetonitrile
I decided to repeat my earlier experiments, beacuse I forget some experimental details and results.
... |
23-11-2016 at 09:41
by: kmno4 |
Need help recovering alpha-phenylacetoacetonitrile
I performed this synthesis in a few runs, with many modifications.
Originally it was given in OS in ... |
10-11-2016 at 02:47
by: kmno4 |
Crystallization of anhydrous sulfates
The most common method of obtaining such compounds in form of (small) crystals is crystallization fr ... |
3-9-2016 at 22:20
by: kmno4 |
Molten potassium thiocyanate
I also did some googling and in 2 minutes (changing keywords) found this: "Advances in Molten Salt C ... |
11-7-2016 at 03:15
by: kmno4 |
Discoloration of Copper Sulfate Pentahydrate by Lithium Chloride
http://lib.dr.iastate.edu/cgi/viewcontent.cgi?article=1207&context=ameslab_iscreports
also:
ht ... |
5-1-2016 at 02:43
by: kmno4 |
Preparation of cyanides
[rquote=419377&tid=23&author=lysander]
Heat solution to 60C.
[/rquote]
The mixture should ... |
16-9-2015 at 10:56
by: kmno4 |
Remarkable reaction of antimony
[quote]I did the experiment with RbCl instead of CsCl, but this was not successful. When a solution ... |
24-4-2015 at 12:34
by: kmno4 |
Remarkable reaction of antimony
I decided to check preparation (given by Wienland) of "(Sb, Sn)CI6(NH4)2".
Equal volumes of solutio ... |
16-4-2015 at 11:41
by: kmno4 |
Remarkable reaction of antimony
Some info about colour of Cs chloroantimonates:
[file]38980[/file]
Some info about spectra Sb( ... |
14-4-2015 at 09:03
by: kmno4 |
Modafinil: its preparation via Bunte salt
Part 2: Oxidation of 2-(benzhydrylthio)acetamide to the sulfoxide
Among preparative methods of ox ... |
1-3-2015 at 23:58
by: kmno4 |
Copper carbonate - controlling the colour
[rquote=390309&tid=50822&author=blogfast25]
Listen you dipshit,... blabla.....[/rquote]
In ... |
3-2-2015 at 11:36
by: kmno4 |
Copper carbonate - controlling the colour
[quote]It outlines the methodology as well as the result: pKs = 31.9, which indicates extremely low ... |
3-2-2015 at 10:44
by: kmno4 |
Does this reaction happen at all?
[rquote=389162&tid=61300&author=blogfast25][rquote=389147&tid=61300&author=kmno4][rq ... |
28-1-2015 at 14:45
by: kmno4 |
Does this reaction happen at all?
[rquote=389128&tid=61300&author=hissingnoise]No, is the short answer ─ as N[sub]2[/sub] bo ... |
27-1-2015 at 14:14
by: kmno4 |
phenylcyclopentylaceticacid synthesis? (and it's esters)
Reaction of phenylacetonitrile with cyclopentyl bromide under PTC conditions will give α-s ... |
24-1-2015 at 00:11
by: kmno4 |
Best non-polar solvent for caffeine
[rquote=388568&tid=61253&author=gdflp]However, if you don't have access to diethyl ether ano ... |
22-1-2015 at 05:32
by: kmno4 |
Is solubility of salts in Acetone predictable?
Is solubility of salts in Acetone predictable ?
Generally - no.
But in cases of singly charged, ... |
22-1-2015 at 05:17
by: kmno4 |
Modafinil: its preparation via Bunte salt
[rquote=387476&tid=61136&author=Nicodem]
[quote]For each 1 mol of sodium thiosulfate*, 1,02 ... |
14-1-2015 at 13:00
by: kmno4 |
Modafinil: its preparation via Bunte salt
There are several synthetic ways to modafinil, more or less complicated, giving various yields of
f ... |
10-1-2015 at 17:32
by: kmno4 |
Hydrolysis and decarboxylation of nitriles with Phosphoric acid. Can't find any experimental data.
Long time ago I made such an experiment with ketonitrile (mentioned earlier in OS procedure).
Wit ... |
11-12-2014 at 14:57
by: kmno4 |
Iron in Molybdenum filament supports
I performed XRF analysis of metallic parts of two light bulbs, from two different manufacturers.
... |
11-12-2014 at 14:37
by: kmno4 |
The Condensation Reaction Of Salicylic Acid And Acetone
[rquote=364293&tid=44955&author=AvBaeyer]
Here is a file from a brief SciFinder search rega ... |
12-11-2014 at 01:48
by: kmno4 |
chemistry of GOLD, known reactions and techniques
As I understand, it is some kind of dirty equipment exhibition, because it has nothing (so far) to d ... |
8-11-2014 at 00:07
by: kmno4 |
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